7-hydroxy-1-<<<4-(3-methoxyphenyl)-1-piperazinyl>acetyl>amino>-2,2,4-trimethylindan hemifumarate

Base Information

Chemical Name:7-hydroxy-1-<<<4-(3-methoxyphenyl)-1-piperazinyl>acetyl>amino>-2,2,4-trimethylindan hemifumarate
CAS No.:103247-39-8
Molecular Formula:C₄H₄O₄*2C₂₅H₃₃N₃O₃
Molecular Weight:963.184
Hs Code.:

Synonyms:7-hydroxy-1-<<<4-(3-methoxyphenyl)-1-piperazinyl>acetyl>amino>-2,2,4-trimethylindan hemifumarate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-hydroxy-1-<<<4-(3-methoxyphenyl)-1-piperazinyl>acetyl>amino>-2,2,4-trimethylindan hemifumarate

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Technology Process of 7-hydroxy-1-<<<4-(3-methoxyphenyl)-1-piperazinyl>acetyl>amino>-2,2,4-trimethylindan hemifumarate

There total 2 articles about 7-hydroxy-1-<<<4-(3-methoxyphenyl)-1-piperazinyl>acetyl>amino>-2,2,4-trimethylindan hemifumarate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 133794-94-2
1-<(chloroacetyl)amino>-7-hydroxy-2,2,4-trimethylindan

: 16015-71-7
4-(3-methoxyphenyl)piperazine

: 103247-39-8
7-hydroxy-1-<<<4-(3-methoxyphenyl)-1-piperazinyl>acetyl>amino>-2,2,4-trimethylindan hemifumarate

Guidance literature:: With triethylamine; In acetonitrile; for 3h; Heating;
DOI:10.1021/jm00111a013

Reference yield:

: 133794-89-5
1-amino-7-hydroxy-2,2,4-trimethylindan

: 103247-39-8
7-hydroxy-1-<<<4-(3-methoxyphenyl)-1-piperazinyl>acetyl>amino>-2,2,4-trimethylindan hemifumarate

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / Et₃N / CHCl₃ / 2 h / 0 °C

2: 78 percent / Et₃N / acetonitrile / 3 h / Heating

With triethylamine; In chloroform; acetonitrile;
DOI:10.1021/jm00111a013