5-((E)-6-{(1S,2R,3S,4R)-3-[(E)-(3R,4S)-4-Phenyl-3-(tetrahydro-pyran-2-yloxy)-pent-1-enyl]-7-oxa-bicyclo[2.2.1]hept-2-yl}-hex-4-enyl)-1H-tetrazole

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Chemical Name:5-((E)-6-{(1S,2R,3S,4R)-3-[(E)-(3R,4S)-4-Phenyl-3-(tetrahydro-pyran-2-yloxy)-pent-1-enyl]-7-oxa-bicyclo[2.2.1]hept-2-yl}-hex-4-enyl)-1H-tetrazole
CAS No.:126295-70-3
Molecular Formula:C₂₉H₄₀N₄O₃
Molecular Weight:492.662
Hs Code.:

Synonyms:5-((E)-6-{(1S,2R,3S,4R)-3-[(E)-(3R,4S)-4-Phenyl-3-(tetrahydro-pyran-2-yloxy)-pent-1-enyl]-7-oxa-bicyclo[2.2.1]hept-2-yl}-hex-4-enyl)-1H-tetrazole

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Chemical Property of 5-((E)-6-{(1S,2R,3S,4R)-3-[(E)-(3R,4S)-4-Phenyl-3-(tetrahydro-pyran-2-yloxy)-pent-1-enyl]-7-oxa-bicyclo[2.2.1]hept-2-yl}-hex-4-enyl)-1H-tetrazole

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Technology Process of 5-((E)-6-{(1S,2R,3S,4R)-3-[(E)-(3R,4S)-4-Phenyl-3-(tetrahydro-pyran-2-yloxy)-pent-1-enyl]-7-oxa-bicyclo[2.2.1]hept-2-yl}-hex-4-enyl)-1H-tetrazole

There total 3 articles about 5-((E)-6-{(1S,2R,3S,4R)-3-[(E)-(3R,4S)-4-Phenyl-3-(tetrahydro-pyran-2-yloxy)-pent-1-enyl]-7-oxa-bicyclo[2.2.1]hept-2-yl}-hex-4-enyl)-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104101-47-5
5,6-Dihydroxy-7-{(1S,2R,3S,4R)-3-[(E)-(3R,4S)-4-phenyl-3-(tetrahydro-pyran-2-yloxy)-pent-1-enyl]-7-oxa-bicyclo[2.2.1]hept-2-yl}-heptanoic acid methyl ester

: 126295-70-3
5-((E)-6-{(1S,2R,3S,4R)-3-[(E)-(3R,4S)-4-Phenyl-3-(tetrahydro-pyran-2-yloxy)-pent-1-enyl]-7-oxa-bicyclo[2.2.1]hept-2-yl}-hex-4-enyl)-1H-tetrazole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium metaperiodate / methanol; H₂O / 2 h / 25 °C

2: 1.) potassium tert-amylate / 1.) THF/toluene, 0 deg C, 1 h, 2.)25 deg C, 1 h

With sodium periodate; potassium 2-methylbutan-2-olate; In methanol; water;
DOI:10.1021/jm00168a032

Reference yield:

: 5,6-Dihydroxy-7-{(1S,2R,3S,4R)-3-[(E)-(3R,4S)-4-phenyl-3-(tetrahydro-pyran-2-yloxy)-pent-1-enyl]-7-oxa-bicyclo[2.2.1]hept-2-yl}-heptanoic acid

: 126295-70-3
5-((E)-6-{(1S,2R,3S,4R)-3-[(E)-(3R,4S)-4-Phenyl-3-(tetrahydro-pyran-2-yloxy)-pent-1-enyl]-7-oxa-bicyclo[2.2.1]hept-2-yl}-hex-4-enyl)-1H-tetrazole

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether

2: sodium metaperiodate / methanol; H₂O / 2 h / 25 °C

3: 1.) potassium tert-amylate / 1.) THF/toluene, 0 deg C, 1 h, 2.)25 deg C, 1 h

With sodium periodate; potassium 2-methylbutan-2-olate; In methanol; diethyl ether; water;
DOI:10.1021/jm00168a032

Reference yield:

: 126451-84-1
1S-<1α,2α,3α(E,3S^*,4R^*),4α>-7-<3-<4-phenyl-3-(tetrahydropyranyloxy)-1-pentenyl>-7-oxabicyclo<2.2.1>hept-2-yl>acetaldehyde

: 42743-15-7
4-(tetrazol-5-yl)-butyltriphenylphosphonium bromide

: 126295-70-3
5-((E)-6-{(1S,2R,3S,4R)-3-[(E)-(3R,4S)-4-Phenyl-3-(tetrahydro-pyran-2-yloxy)-pent-1-enyl]-7-oxa-bicyclo[2.2.1]hept-2-yl}-hex-4-enyl)-1H-tetrazole

Guidance literature:: With potassium 2-methylbutan-2-olate; Yield given. Multistep reaction; 1.) THF/toluene, 0 deg C, 1 h, 2.)25 deg C, 1 h;
DOI:10.1021/jm00168a032