(-)-(4S,5E/Z)-4-(dibenzylamino)-6-phenylhex-5-enyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

Base Information

Chemical Name:(-)-(4S,5E/Z)-4-(dibenzylamino)-6-phenylhex-5-enyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate
CAS No.:205067-99-8
Molecular Formula:C₃₄H₄₂N₂O₃
Molecular Weight:526.719
Hs Code.:

Synonyms:(-)-(4S,5E/Z)-4-(dibenzylamino)-6-phenylhex-5-enyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

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Chemical Property of (-)-(4S,5E/Z)-4-(dibenzylamino)-6-phenylhex-5-enyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

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Technology Process of (-)-(4S,5E/Z)-4-(dibenzylamino)-6-phenylhex-5-enyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

There total 1 articles about (-)-(4S,5E/Z)-4-(dibenzylamino)-6-phenylhex-5-enyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1449-46-3
benzyltriphenylphosphonium bromide

: 253882-19-8
(+)-(S)-4-(N,N-dibenzylamino)-5-oxopentyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

: 205067-99-8
(-)-(4S,5E/Z)-4-(dibenzylamino)-6-phenylhex-5-enyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

Guidance literature:: With potassium tert-butylate; In diethyl ether; at -18 - 20 ℃;
DOI:10.1002/(SICI)1522-2675(19991110)82:11<1860::AID-HLCA1860>3.0.CO;2-8

Reference yield: 70.0%

: 205067-99-8
(-)-(4S,5E/Z)-4-(dibenzylamino)-6-phenylhex-5-enyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

: (-)-(1R,2R,3S)-2[(R/S)-(deutero)(phenyl)methyl]-3-(dibenzylamino)cyclopentyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

Guidance literature:: (-)-(4S,5E/Z)-4-(dibenzylamino)-6-phenylhex-5-enyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate; With sec.-butyllithium; (-)-sparteine; In diethyl ether; at -78 ℃; for 18h;

With deuteromethanol; In diethyl ether; at -78 - 20 ℃;
DOI:10.1002/(SICI)1522-2675(19991110)82:11<1860::AID-HLCA1860>3.0.CO;2-8

Reference yield: 70.0%

: 205067-99-8
(-)-(4S,5E/Z)-4-(dibenzylamino)-6-phenylhex-5-enyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

: 2,2,4,4-Tetramethyl-oxazolidine-3-carboxylic acid (1R,2R,3S)-2-benzyl-3-dibenzylamino-cyclopentyl ester

Guidance literature:: With methanol; sec.-butyllithium; (-)-sparteine; 1.) Et2O, -78 deg C, 18 h; 2.) Et2O, -78 deg C -> room temp.;
DOI:10.1016/S0040-4039(98)00085-9