methyl (2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Base Information

• Chemical Name: methyl (2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside
• CAS No.: 635321-20-9
• Molecular Formula: C₆₂H₆₀O₁₄
• Molecular Weight: 1029.15

Synonyms:methyl (2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

Chemical Property of methyl (2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

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Technology Process of methyl (2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside

There total 27 articles about methyl (2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

methyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside (34234-44-1,53182-61-9,88037-32-5,101194-17-6,120104-44-1,120104-49-6) + 1-ethynylcyclohexyl 2,3,4,6-tetra-O-benzyl α-D-mannopyranoside (1384752-77-5) → methyl (2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside (635321-20-9)

Guidance literature:

With gold(III) chloride; silver hexafluoroantimonate; In dichloromethane; acetonitrile; at 25 ℃; for 4h; Inert atmosphere;

DOI:10.1039/c2cc32649c

Reference yield: 61.0%

methyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside (34234-44-1,53182-61-9,88037-32-5,101194-17-6,120104-44-1,120104-49-6) + (2R,3R,4S,5S,6S)-3,4,5-tris(benzyloxy)-2-((benzyloxy)methyl)-6-methoxytetrahydro-2H-pyran (3879-79-6,17791-37-6,19488-61-0,53008-63-2,69237-94-1,69237-95-2,71526-33-5,83462-67-3,84799-77-9,103421-29-0,103421-30-3,139241-42-2,61330-62-9) → methyl (2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside (635321-20-9)

Guidance literature:

With gold(III) tribromide; In acetonitrile; at 70 ℃; for 24h; Inert atmosphere;

DOI:10.1039/b822526e

Reference yield: 18.0%

methyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside (34234-44-1,53182-61-9,88037-32-5,101194-17-6,120104-44-1,120104-49-6) + 2-propynyl 2,3,4,6-tetra-O-benzyl-α-D-mannopyranoside → methyl (2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-α-D-mannopyranoside (635321-20-9)

Guidance literature:

With gold(III) chloride; In acetonitrile; at 25 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c2cc32649c

upstream raw materials:

methyl 2,3,4-tri-O-benzoylglucopyranoside

S-ethyl 2,3,4,6-tetra-O-benzyl-1-deoxy-1-thio-α-D-mannopyranoside

methyl 2,3,4-tri-O-benzoyl-α-D-mannopyranoside

2,3,4,6-tetra-O-benzyl-α-mannopyranosyl benzyl phthalate

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