dimethyl 2,2'-[naphthalene-1,7-diylbis(3-benzyloxy-5-oxofuran-4-yl-2-ylidene)]bis[(4-benzyloxyphenyl)acetate]

Base Information

Chemical Name:dimethyl 2,2'-[naphthalene-1,7-diylbis(3-benzyloxy-5-oxofuran-4-yl-2-ylidene)]bis[(4-benzyloxyphenyl)acetate]
CAS No.:887259-54-3
Molecular Formula:C₆₄H₄₈O₁₂
Molecular Weight:1009.08
Hs Code.:

Synonyms:dimethyl 2,2'-[naphthalene-1,7-diylbis(3-benzyloxy-5-oxofuran-4-yl-2-ylidene)]bis[(4-benzyloxyphenyl)acetate]

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Chemical Property of dimethyl 2,2'-[naphthalene-1,7-diylbis(3-benzyloxy-5-oxofuran-4-yl-2-ylidene)]bis[(4-benzyloxyphenyl)acetate]

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Technology Process of dimethyl 2,2'-[naphthalene-1,7-diylbis(3-benzyloxy-5-oxofuran-4-yl-2-ylidene)]bis[(4-benzyloxyphenyl)acetate]

There total 1 articles about dimethyl 2,2'-[naphthalene-1,7-diylbis(3-benzyloxy-5-oxofuran-4-yl-2-ylidene)]bis[(4-benzyloxyphenyl)acetate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 887259-45-2
methyl {3-benzyloxy-5-oxo-4-[(trifluoromethylsulfonyl)oxy]furan-2(5H)-ylidene}(4-benzyloxyphenyl)acetate

: 561015-09-6
2,2'-naphthalene-1,7-diyl(4,4,5,5-tetramethyl-1,3,2-dioxoborolane)

: 887259-54-3
dimethyl 2,2'-[naphthalene-1,7-diylbis(3-benzyloxy-5-oxofuran-4-yl-2-ylidene)]bis[(4-benzyloxyphenyl)acetate]

Guidance literature:: With sodium carbonate; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; for 3h; Heating;
DOI:10.1002/ejoc.200500837

Reference yield: 90.0%

: 887259-54-3
dimethyl 2,2'-[naphthalene-1,7-diylbis(3-benzyloxy-5-oxofuran-4-yl-2-ylidene)]bis[(4-benzyloxyphenyl)acetate]

: dimethyl 2,2'-[naphthalene-1,7-diylbis(3-hydroxy-5-oxofuran-4-yl-2-ylidene)]bis[(4-hydroxyphenyl)acetate]

Guidance literature:: With hydrogen; palladium on activated charcoal; In dichloromethane; at 20 ℃; for 26h;
DOI:10.1002/ejoc.200500837

Reference yield:

: 887259-54-3
dimethyl 2,2'-[naphthalene-1,7-diylbis(3-benzyloxy-5-oxofuran-4-yl-2-ylidene)]bis[(4-benzyloxyphenyl)acetate]

: 2,2'-[naphthalene-1,7-diylbis(3-hydroxy-5-oxofuran-4-yl-2-ylidene)]bis[(4-hydroxyphenyl)acetic acid]

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / hydrogen / Pd/C / CH₂Cl₂ / 26 h / 20 °C

2: 90 percent / NaOH / H₂O / 1 h / 100 °C

With sodium hydroxide; hydrogen; palladium on activated charcoal; In dichloromethane; water;
DOI:10.1002/ejoc.200500837