ethyl syn-3-(1-(benzyloxy)-2,2-dimethylpropyl)-2-(ethoxycarbonyl)heptanoate

Base Information

Chemical Name:ethyl syn-3-(1-(benzyloxy)-2,2-dimethylpropyl)-2-(ethoxycarbonyl)heptanoate
CAS No.:143372-36-5
Molecular Formula:C₂₄H₃₈O₅
Molecular Weight:406.563
Hs Code.:

Synonyms:ethyl syn-3-(1-(benzyloxy)-2,2-dimethylpropyl)-2-(ethoxycarbonyl)heptanoate

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Chemical Property of ethyl syn-3-(1-(benzyloxy)-2,2-dimethylpropyl)-2-(ethoxycarbonyl)heptanoate

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Technology Process of ethyl syn-3-(1-(benzyloxy)-2,2-dimethylpropyl)-2-(ethoxycarbonyl)heptanoate

There total 8 articles about ethyl syn-3-(1-(benzyloxy)-2,2-dimethylpropyl)-2-(ethoxycarbonyl)heptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 143372-32-1
ethyl 4-(benzyloxy)-5,5-dimethyl-2-(ethoxycarbonyl)-2-hexenoate

: 143372-36-5
ethyl syn-3-(1-(benzyloxy)-2,2-dimethylpropyl)-2-(ethoxycarbonyl)heptanoate

Guidance literature:: In diethyl ether; at -30 ℃; for 2h;

Reference yield: 99.0%

: 68079-35-6
CH₃CH₂CH₂CH₂Cu*BF₃

: 143372-32-1
ethyl 4-(benzyloxy)-5,5-dimethyl-2-(ethoxycarbonyl)-2-hexenoate

: 143372-36-5
ethyl syn-3-(1-(benzyloxy)-2,2-dimethylpropyl)-2-(ethoxycarbonyl)heptanoate

Guidance literature:: In diethyl ether; at -30 ℃; for 2h;

Reference yield:

: 59562-82-2
3,3-dimetylbutan-1,2-diol

: 143372-36-5
ethyl syn-3-(1-(benzyloxy)-2,2-dimethylpropyl)-2-(ethoxycarbonyl)heptanoate

Guidance literature:: Multi-step reaction with 6 steps

1: DMAP, Et₃N / dimethylformamide / 48 h / Ambient temperature

2: 1.) NaH / 1.) THF, 24 h, 2.) THF, 2 d

3: TsOH / methanol / 8 h / 80 °C

4: 1.) oxalyl chloride, DMSO, 2.) Et₃N / 1.) CH₂Cl₂, -78 deg C, 45 min, 2.)CH₂Cl₂, 0 deg C, overnight

5: 88.1 percent / TiCl₄, pyridine / tetrahydrofuran / 48 h / Ambient temperature

6: 99 percent / diethyl ether / 2 h / -30 °C

With pyridine; dmap; oxalyl dichloride; titanium tetrachloride; sodium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; diethyl ether; N,N-dimethyl-formamide;