6-(acetylamino)-7-nitro-1-<<4-(phenylsulfonyl)phenyl>thio>-1,2,3,4-tetrahydronaphthalene

Base Information

Chemical Name:6-(acetylamino)-7-nitro-1-<<4-(phenylsulfonyl)phenyl>thio>-1,2,3,4-tetrahydronaphthalene
CAS No.:138814-34-3
Molecular Formula:C₂₄H₂₂N₂O₅S₂
Molecular Weight:482.581
Hs Code.:

Synonyms:6-(acetylamino)-7-nitro-1-<<4-(phenylsulfonyl)phenyl>thio>-1,2,3,4-tetrahydronaphthalene

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Chemical Property of 6-(acetylamino)-7-nitro-1-<<4-(phenylsulfonyl)phenyl>thio>-1,2,3,4-tetrahydronaphthalene

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Technology Process of 6-(acetylamino)-7-nitro-1-<<4-(phenylsulfonyl)phenyl>thio>-1,2,3,4-tetrahydronaphthalene

There total 4 articles about 6-(acetylamino)-7-nitro-1-<<4-(phenylsulfonyl)phenyl>thio>-1,2,3,4-tetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 117013-78-2
6-(acetylamino)-7-nitro-1,2,3,4-tetrahydronaphthalen-1-one

: 138814-34-3
6-(acetylamino)-7-nitro-1-<<4-(phenylsulfonyl)phenyl>thio>-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / NaBH₄ / methanol / 1 h / 25 °C

2: HCl(gas) / benzene / 0.08 h

3: 1.) NaH / 1.) DMF, 25 deg C, 1 h, 2.) DMF, -43 deg C, 2 h

With hydrogenchloride; sodium tetrahydroborate; sodium hydride; In methanol; benzene;
DOI:10.1021/jm00083a007

Reference yield:

: 138814-32-1
6-(acetylamino)-7-nitro-1,2,3,4-tetrahydronaphthalen-1-ol

: 138814-34-3
6-(acetylamino)-7-nitro-1-<<4-(phenylsulfonyl)phenyl>thio>-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: HCl(gas) / benzene / 0.08 h

2: 1.) NaH / 1.) DMF, 25 deg C, 1 h, 2.) DMF, -43 deg C, 2 h

With hydrogenchloride; sodium hydride; In benzene;
DOI:10.1021/jm00083a007

Reference yield:

: 88611-67-0
6-acetamido-1,2,3,4-tetrahydronaphthalen-1-one

: 138814-34-3
6-(acetylamino)-7-nitro-1-<<4-(phenylsulfonyl)phenyl>thio>-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 4 steps

1: 3.85 g / concd. nitric acid / acetic acid / a) 0 deg C, 2 h, b) 25 deg C, 2 h

2: 89 percent / NaBH₄ / methanol / 1 h / 25 °C

3: HCl(gas) / benzene / 0.08 h

4: 1.) NaH / 1.) DMF, 25 deg C, 1 h, 2.) DMF, -43 deg C, 2 h

With hydrogenchloride; sodium tetrahydroborate; nitric acid; sodium hydride; In methanol; acetic acid; benzene;
DOI:10.1021/jm00083a007