[4-Methyl-3-((3E,7E)-7-methyl-trideca-3,7-dien-11-ynyl)-cyclohex-3-enyloxymethyl]-benzene

Base Information

Chemical Name:[4-Methyl-3-((3E,7E)-7-methyl-trideca-3,7-dien-11-ynyl)-cyclohex-3-enyloxymethyl]-benzene
CAS No.:85221-05-2
Molecular Formula:C₂₈H₃₈O
Molecular Weight:390.609
Hs Code.:

Synonyms:[4-Methyl-3-((3E,7E)-7-methyl-trideca-3,7-dien-11-ynyl)-cyclohex-3-enyloxymethyl]-benzene

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Chemical Property of [4-Methyl-3-((3E,7E)-7-methyl-trideca-3,7-dien-11-ynyl)-cyclohex-3-enyloxymethyl]-benzene

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Technology Process of [4-Methyl-3-((3E,7E)-7-methyl-trideca-3,7-dien-11-ynyl)-cyclohex-3-enyloxymethyl]-benzene

There total 8 articles about [4-Methyl-3-((3E,7E)-7-methyl-trideca-3,7-dien-11-ynyl)-cyclohex-3-enyloxymethyl]-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 41143-17-3
(E)-4-methyldec-4-en-8-ynal

: 85221-03-0
[3-(5-Benzyloxy-2-methyl-cyclohex-1-enyl)-propylidene]-triphenyl-λ⁵-phosphane

: 85221-05-2
[4-Methyl-3-((3E,7E)-7-methyl-trideca-3,7-dien-11-ynyl)-cyclohex-3-enyloxymethyl]-benzene

Guidance literature:: In tetrahydrofuran; diethyl ether; at -78 - -30 ℃;
DOI:10.1021/ja00346a073

Reference yield:

: 41143-16-2
methyl-2 octene-1 yne-6 ol-3

: 85221-05-2
[4-Methyl-3-((3E,7E)-7-methyl-trideca-3,7-dien-11-ynyl)-cyclohex-3-enyloxymethyl]-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / Hg(OAc)2

2: 52 percent / diethyl ether; tetrahydrofuran / -78 - -30 °C

With mercury(II) diacetate; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja00346a073

Reference yield:

: 73658-27-2
4-Benzyloxy-1-methyl-2-methylene-cyclohexanol

: 85221-05-2
[4-Methyl-3-((3E,7E)-7-methyl-trideca-3,7-dien-11-ynyl)-cyclohex-3-enyloxymethyl]-benzene

Guidance literature:: Multi-step reaction with 7 steps

1: 62 percent / Hg(OAc)2 / Heating

2: 92 percent / LiAlH₄ / diethyl ether / 0 °C

3: pyridine / 0 °C

4: LiBr / acetone / Heating

5: benzene / Heating

6: C₆H₅Li / diethyl ether; tetrahydrofuran / Ambient temperature

7: 52 percent / diethyl ether; tetrahydrofuran / -78 - -30 °C

With pyridine; lithium aluminium tetrahydride; mercury(II) diacetate; phenyllithium; lithium bromide; In tetrahydrofuran; diethyl ether; acetone; benzene;
DOI:10.1021/ja00346a073