naphthalene-1-sulfinic acid phenylamide

Base Information

• Chemical Name: naphthalene-1-sulfinic acid phenylamide
• CAS No.: 38270-79-0
• Molecular Formula: C₁₆H₁₃NOS
• Molecular Weight: 267.351
• Mol file: 38270-79-0.mol

Synonyms:naphthalene-1-sulfinic acid phenylamide

Chemical Property of naphthalene-1-sulfinic acid phenylamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of naphthalene-1-sulfinic acid phenylamide

There total 2 articles about naphthalene-1-sulfinic acid phenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

aniline (62-53-3) + 1-(2-methylpropane-2-sulfinyl)naphthalene (153483-49-9) → naphthalene-1-sulfinic acid phenylamide (38270-79-0)

Guidance literature:

1-(2-methylpropane-2-sulfinyl)naphthalene; With N-Bromosuccinimide; acetic acid; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;

aniline; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;

DOI:10.1021/acs.orglett.5b02743

Reference yield:

→ naphthalene-1-sulfinic acid phenylamide (38270-79-0)

Guidance literature:

α-Bromnaphthalin, N-Sulfinylanilin;

DOI:10.1021/ja00770a047

upstream raw materials:

aniline

1-(2-methylpropane-2-sulfinyl)naphthalene