Technology Process of C29H37FN4O2
There total 7 articles about C29H37FN4O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridine / dichloromethane / -10 - 20 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride; tert-butyl alcohol / acetonitrile / 1.5 h / 70 °C
3: potassium hydroxide / methanol / Reflux
4: thionyl chloride / acetonitrile / 70 °C / Inert atmosphere
5: triethylamine / acetonitrile / 0.5 h / 20 °C
6: water; sodium hydrogencarbonate / methanol / 2 h / 50 °C
With
pyridine; thionyl chloride; tetrabutyl ammonium fluoride; water; sodium hydrogencarbonate; triethylamine; potassium hydroxide; tert-butyl alcohol;
In
methanol; dichloromethane; acetonitrile;
DOI:10.1016/j.ejmech.2011.06.023
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetrabutyl ammonium fluoride; tert-butyl alcohol / acetonitrile / 1.5 h / 70 °C
2: potassium hydroxide / methanol / Reflux
3: thionyl chloride / acetonitrile / 70 °C / Inert atmosphere
4: triethylamine / acetonitrile / 0.5 h / 20 °C
5: water; sodium hydrogencarbonate / methanol / 2 h / 50 °C
With
thionyl chloride; tetrabutyl ammonium fluoride; water; sodium hydrogencarbonate; triethylamine; potassium hydroxide; tert-butyl alcohol;
In
methanol; acetonitrile;
DOI:10.1016/j.ejmech.2011.06.023