3-isopropyl-N⁽⁶⁾-tosylsydnonimine

Base Information

Chemical Name:3-isopropyl-N⁽⁶⁾-tosylsydnonimine
CAS No.:1252634-32-4
Molecular Formula:C₁₂H₁₅N₃O₃S
Molecular Weight:281.335
Hs Code.:

3-isopropyl-N<sup>(6)</sup>-tosylsydnonimine

Synonyms:3-isopropyl-N⁽⁶⁾-tosylsydnonimine

Suppliers and Price of 3-isopropyl-N⁽⁶⁾-tosylsydnonimine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-isopropyl-N⁽⁶⁾-tosylsydnonimine

Chemical Property:

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Technology Process of 3-isopropyl-N⁽⁶⁾-tosylsydnonimine

There total 1 articles about 3-isopropyl-N⁽⁶⁾-tosylsydnonimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 5123-98-8
3-isopropylsydnone imine hydrochloride

: 98-59-9
p-toluenesulfonyl chloride

: 1252634-32-4
3-isopropyl-N⁽⁶⁾-tosylsydnonimine

Guidance literature:: With triethylamine; In dichloromethane; at -20 - 20 ℃; for 17.5h;
DOI:10.1007/s11172-009-0346-2

Reference yield: 83.0%

: 1252634-32-4
3-isopropyl-N⁽⁶⁾-tosylsydnonimine

: 21511-55-7,34643-89-5
(methoxymethylidene)dimethylammonium methyl sulfate

: 1252634-40-4
4-formyl-3-isopropyl-N₆-tosylsydnone imine

Guidance literature:: 3-isopropyl-N⁽⁶⁾-tosylsydnonimine; With n-butyllithium; In tetrahydrofuran; hexane; at -90 ℃; for 0.666667h; Inert atmosphere;

(methoxymethylidene)dimethylammonium methyl sulfate; In tetrahydrofuran; hexane; at -90 - 20 ℃; Inert atmosphere;

With water; sodium hydrogencarbonate; In tetrahydrofuran; hexane; at 20 ℃;
DOI:10.1007/s11172-009-0346-2

Reference yield:

: 1252634-32-4
3-isopropyl-N⁽⁶⁾-tosylsydnonimine

: 104-88-1
4-chlorobenzaldehyde

: 4-[(4'-chlorophenyl)hydroxymethyl]-3-isopropyl-N₆-tosylsydnone imine

Guidance literature:: 3-isopropyl-N⁽⁶⁾-tosylsydnonimine; With n-butyllithium; In tetrahydrofuran; hexane; at -80 ℃; for 0.166667h; Inert atmosphere;

4-chlorobenzaldehyde; In tetrahydrofuran; hexane; at -80 - 20 ℃; for 0.416667h; Reagent/catalyst; Inert atmosphere;
DOI:10.1016/j.jorganchem.2021.121841