ethyl trans-1-(3,4,5-trimethoxyphenacyl)-5-ethyl-2-oxo-4-piperidineacetate

Base Information

Chemical Name:ethyl trans-1-(3,4,5-trimethoxyphenacyl)-5-ethyl-2-oxo-4-piperidineacetate
CAS No.:56774-75-5
Molecular Formula:C₂₂H₃₁NO₇
Molecular Weight:421.491
Hs Code.:

Synonyms:ethyl trans-1-(3,4,5-trimethoxyphenacyl)-5-ethyl-2-oxo-4-piperidineacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl trans-1-(3,4,5-trimethoxyphenacyl)-5-ethyl-2-oxo-4-piperidineacetate

Chemical Property:

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Technology Process of ethyl trans-1-(3,4,5-trimethoxyphenacyl)-5-ethyl-2-oxo-4-piperidineacetate

There total 1 articles about ethyl trans-1-(3,4,5-trimethoxyphenacyl)-5-ethyl-2-oxo-4-piperidineacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 51490-01-8
1-(3,4,5-trimethoxyphenyl)-2-bromoethanone

: 56774-65-3,96790-30-6,96790-31-7,97673-06-8,109009-07-6
((3S,4S)-6-Ethoxy-3-ethyl-2,3,4,5-tetrahydro-pyridin-4-yl)-acetic acid ethyl ester

: 56774-75-5
ethyl trans-1-(3,4,5-trimethoxyphenacyl)-5-ethyl-2-oxo-4-piperidineacetate

Guidance literature:: In N,N-dimethyl-formamide; at 60 ℃; for 6h;
DOI:10.1016/0040-4020(80)80049-4

Reference yield: 100.0%

: 56774-75-5
ethyl trans-1-(3,4,5-trimethoxyphenacyl)-5-ethyl-2-oxo-4-piperidineacetate

: 74627-65-9,74627-66-0
ethyl trans-1-<2-(3,4,5-trimethoxyphenyl)-2-hydroxyethyl>-5-ethyl-2-oxo-4-piperidineacetate

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 1.5h; Ambient temperature;
DOI:10.1016/0040-4020(80)80049-4

Reference yield:

: 56774-75-5
ethyl trans-1-(3,4,5-trimethoxyphenacyl)-5-ethyl-2-oxo-4-piperidineacetate

: 74627-67-1
ethyl trans-1-(3,4,5-trimethoxyphenethyl)-5-ethyl-2-oxo-4-piperidineacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaBH₄ / ethanol / 1.5 h / Ambient temperature

2: 68 percent / 70percent aq. HClO₄, H₂ / 10percent Pd/C / ethanol / 20 h / 28 °C / 3040 Torr

With sodium tetrahydroborate; perchloric acid; hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1016/0040-4020(80)80049-4