(Diisopropoxy-phosphoryl)-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

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Chemical Name:(Diisopropoxy-phosphoryl)-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester
CAS No.:113368-90-4
Molecular Formula:C₂₄H₃₉O₅P
Molecular Weight:438.544
Hs Code.:

Synonyms:(Diisopropoxy-phosphoryl)-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

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Chemical Property of (Diisopropoxy-phosphoryl)-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

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Technology Process of (Diisopropoxy-phosphoryl)-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

There total 1 articles about (Diisopropoxy-phosphoryl)-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 72946-10-2
diisopropyl (methoxycarbonylmethyl)phosphonate

: 65253-04-5
(-)-8-phenylmenthol

: 113368-90-4
(Diisopropoxy-phosphoryl)-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Guidance literature:: With dmap; In toluene; for 120h; Heating;
DOI:10.1016/S0040-4039(00)96188-4

Reference yield: 84.0%

: 113368-90-4
(Diisopropoxy-phosphoryl)-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

: 1-(Diphenyl-phosphinoyl)-piperidine-2-carbaldehyde

: (E)-3-[1-(Diphenyl-phosphinoyl)-piperidin-2-yl]-acrylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Guidance literature:: With 18-crown-6 ether; potassium hexamethylsilazane; In tetrahydrofuran; at -78 ℃;
DOI:10.1016/S0040-4039(97)10428-2

Reference yield: 55.0%

: 113368-90-4
(Diisopropoxy-phosphoryl)-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

: 300578-89-6
meso-(2R,5S)-2,5-bis(2,2-dimethylpropionyloxy)hexane-1,6-dial

: 300578-90-9
(E)-(4R,7S)-4,7-bis(2,2-dimethylpropionyloxy)-8-oxoocta-2-enoic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester

: (2E,8E)-(4S,7R)-4,7-Bis-(2,2-dimethyl-propionyloxy)-deca-2,8-dienedioic acid bis-[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl] ester

Guidance literature:: (Diisopropoxy-phosphoryl)-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester; With 18-crown-6 ether; potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 ℃; for 0.5h;

meso-(2R,5S)-2,5-bis(2,2-dimethylpropionyloxy)hexane-1,6-dial; In tetrahydrofuran; toluene; at -85 ℃; Further stages.;
DOI:10.1021/jo0259111