N-{(2R,3R,4R,5S,6R)-2-Benzyloxy-4-[(2S,3R,4S,5R,6R)-4,5-dihydroxy-6-methyl-3-((2S,3S,4R,5S,6S)-3,4,5-trihydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl}-acetamide

Base Information

Chemical Name:N-{(2R,3R,4R,5S,6R)-2-Benzyloxy-4-[(2S,3R,4S,5R,6R)-4,5-dihydroxy-6-methyl-3-((2S,3S,4R,5S,6S)-3,4,5-trihydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl}-acetamide
CAS No.:130572-19-9
Molecular Formula:C₂₇H₄₁NO₁₄
Molecular Weight:603.621
Hs Code.:

N-{(2R,3R,4R,5S,6R)-2-Benzyloxy-4-[(2S,3R,4S,5R,6R)-4,5-dihydroxy-6-methyl-3-((2S,3S,4R,5S,6S)-3,4,5-trihydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl}-acetamide

Synonyms:N-{(2R,3R,4R,5S,6R)-2-Benzyloxy-4-[(2S,3R,4S,5R,6R)-4,5-dihydroxy-6-methyl-3-((2S,3S,4R,5S,6S)-3,4,5-trihydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl}-acetamide

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Chemical Property of N-{(2R,3R,4R,5S,6R)-2-Benzyloxy-4-[(2S,3R,4S,5R,6R)-4,5-dihydroxy-6-methyl-3-((2S,3S,4R,5S,6S)-3,4,5-trihydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl}-acetamide

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Technology Process of N-{(2R,3R,4R,5S,6R)-2-Benzyloxy-4-[(2S,3R,4S,5R,6R)-4,5-dihydroxy-6-methyl-3-((2S,3S,4R,5S,6S)-3,4,5-trihydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl}-acetamide

There total 5 articles about N-{(2R,3R,4R,5S,6R)-2-Benzyloxy-4-[(2S,3R,4S,5R,6R)-4,5-dihydroxy-6-methyl-3-((2S,3S,4R,5S,6S)-3,4,5-trihydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl}-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.9%

: 130572-18-8
C₃₆H₅₃NO₁₄

: 130572-19-9
N-{(2R,3R,4R,5S,6R)-2-Benzyloxy-4-[(2S,3R,4S,5R,6R)-4,5-dihydroxy-6-methyl-3-((2S,3S,4R,5S,6S)-3,4,5-trihydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl}-acetamide

Guidance literature:: With acetic acid; at 60 ℃;
DOI:10.1016/S0040-4039(00)97612-3

Reference yield:

: 114853-38-2
methyl 1-thio-β-L-fucopyranoside

: 130572-19-9
N-{(2R,3R,4R,5S,6R)-2-Benzyloxy-4-[(2S,3R,4S,5R,6R)-4,5-dihydroxy-6-methyl-3-((2S,3S,4R,5S,6S)-3,4,5-trihydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl}-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 96.8 percent / p-toluenesulfonic acid / dimethylformamide

2: NaH, DMF

3: 60.3 percent / CuBr₂, Bu₄NBr, DDQ, CH₂Cl₂

4: 77.9 percent / 60percent aq.AcOH / 60 °C

With dichloromethane; tetrabutylammomium bromide; sodium hydride; toluene-4-sulfonic acid; acetic acid; N,N-dimethyl-formamide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; copper(ll) bromide; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)97612-3

Reference yield:

: 130572-04-2
methyl 3,4-O-isopropylidene-1-thio-β-L-fucopyranoside

: 130572-19-9
N-{(2R,3R,4R,5S,6R)-2-Benzyloxy-4-[(2S,3R,4S,5R,6R)-4,5-dihydroxy-6-methyl-3-((2S,3S,4R,5S,6S)-3,4,5-trihydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl}-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: NaH, DMF

2: 60.3 percent / CuBr₂, Bu₄NBr, DDQ, CH₂Cl₂

3: 77.9 percent / 60percent aq.AcOH / 60 °C

With dichloromethane; tetrabutylammomium bromide; sodium hydride; acetic acid; N,N-dimethyl-formamide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; copper(ll) bromide;
DOI:10.1016/S0040-4039(00)97612-3