fluoro-mesitylphosphino-tris(trimethylsilyl)methylborane

Base Information

• Chemical Name: fluoro-mesitylphosphino-tris(trimethylsilyl)methylborane
• CAS No.: 1007126-59-1
• Molecular Formula: C₁₉H₃₉BFPSi₃
• Molecular Weight: 412.558
• Mol file: 1007126-59-1.mol

Synonyms:fluoro-mesitylphosphino-tris(trimethylsilyl)methylborane

Chemical Property of fluoro-mesitylphosphino-tris(trimethylsilyl)methylborane

Chemical Property:

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Technology Process of fluoro-mesitylphosphino-tris(trimethylsilyl)methylborane

There total 1 articles about fluoro-mesitylphosphino-tris(trimethylsilyl)methylborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

difluoro{tris(trimethylsilyl)methyl}borane (124408-71-5) + lithium 2,4,6-trimethylphenylhydrophosphanide (89634-37-7,147285-62-9) → fluoro-mesitylphosphino-tris(trimethylsilyl)methylborane (1007126-59-1) + mesitylphosphine (68357-98-2)

Guidance literature:

In hexane; byproducts: LiF; under Ar or N2, 1 equiv. of Li-compd. was added in hexane to hexane soln. of B-compd. at -60 °C, stirring for 30 min, warming to room temp.; soln. was filtered, evapd. in vac., crystn. from a min. amt. of hexane between -25 and -30 °C, elem. anal.;

DOI:10.1002/zaac.200600335

upstream raw materials:

difluoro{tris(trimethylsilyl)methyl}borane

lithium 2,4,6-trimethylphenylhydrophosphanide