4-{p-[N,N'-bis(tert-butoxycarbonyl)-N'-(phenyl)]phenylenediamino}phenyl-6-phenyl-2,2'-bipyridine

Base Information

Chemical Name:4-{p-[N,N'-bis(tert-butoxycarbonyl)-N'-(phenyl)]phenylenediamino}phenyl-6-phenyl-2,2'-bipyridine
CAS No.:1142955-67-6
Molecular Formula:C₄₄H₄₂N₄O₄
Molecular Weight:690.842
Hs Code.:

Synonyms:4-{p-[N,N'-bis(tert-butoxycarbonyl)-N'-(phenyl)]phenylenediamino}phenyl-6-phenyl-2,2'-bipyridine

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Chemical Property of 4-{p-[N,N'-bis(tert-butoxycarbonyl)-N'-(phenyl)]phenylenediamino}phenyl-6-phenyl-2,2'-bipyridine

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Technology Process of 4-{p-[N,N'-bis(tert-butoxycarbonyl)-N'-(phenyl)]phenylenediamino}phenyl-6-phenyl-2,2'-bipyridine

There total 3 articles about 4-{p-[N,N'-bis(tert-butoxycarbonyl)-N'-(phenyl)]phenylenediamino}phenyl-6-phenyl-2,2'-bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 24424-99-5
di-tert-butyl dicarbonate

: C₃₉H₃₄N₄O₂

: 1142955-67-6
4-{p-[N,N'-bis(tert-butoxycarbonyl)-N'-(phenyl)]phenylenediamino}phenyl-6-phenyl-2,2'-bipyridine

Guidance literature:: With dmap; In tetrahydrofuran; for 24h; Reflux;
DOI:10.1021/acs.inorgchem.5b00756

Reference yield:

: 586400-17-1
4-(p-bromophenyl)-6-phenyl-2,2′-bipyridine

: 1142955-67-6
4-{p-[N,N'-bis(tert-butoxycarbonyl)-N'-(phenyl)]phenylenediamino}phenyl-6-phenyl-2,2'-bipyridine

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate / toluene / 9 h / 80 °C / Inert atmosphere

2: dmap / tetrahydrofuran / 24 h / Reflux

With dmap; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate; In tetrahydrofuran; toluene;
DOI:10.1021/acs.inorgchem.5b00756

Reference yield:

: 409357-04-6
N′-(tert-butoxycarbonyl)-N′-(phenyl)-p-phenylenediamine

: 1142955-67-6
4-{p-[N,N'-bis(tert-butoxycarbonyl)-N'-(phenyl)]phenylenediamino}phenyl-6-phenyl-2,2'-bipyridine

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate / toluene / 9 h / 80 °C / Inert atmosphere

2: dmap / tetrahydrofuran / 24 h / Reflux

With dmap; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate; In tetrahydrofuran; toluene;
DOI:10.1021/acs.inorgchem.5b00756