C₃₇H₂₉N₂O₂⁽¹⁺⁾*Cl^(1-)

Base Information

Chemical Name:C₃₇H₂₉N₂O₂⁽¹⁺⁾*Cl^(1-)
CAS No.:1414888-81-5
Molecular Formula:C₃₇H₂₉N₂O₂*Cl
Molecular Weight:569.102
Hs Code.:

C<sub>37</sub>H<sub>29</sub>N<sub>2</sub>O<sub>2</sub><sup>(1+)</sup>*Cl<sup>(1-)</sup>

Synonyms:C₃₇H₂₉N₂O₂⁽¹⁺⁾*Cl^(1-)

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Chemical Property of C₃₇H₂₉N₂O₂⁽¹⁺⁾*Cl^(1-)

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Technology Process of C₃₇H₂₉N₂O₂⁽¹⁺⁾*Cl^(1-)

There total 5 articles about C₃₇H₂₉N₂O₂⁽¹⁺⁾*Cl^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1414888-87-1
C₃₆H₃₀N₂O₂

: 122-51-0
orthoformic acid triethyl ester

: 1414888-81-5
C₃₇H₂₉N₂O₂⁽¹⁺⁾*Cl^(1-)

Guidance literature:: C₃₆H₃₀N₂O₂; With hydrogenchloride; In 1,4-dioxane; dichloromethane; for 2h; Inert atmosphere;

orthoformic acid triethyl ester; at 125 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.09.116 DOI:10.1016/j.tetlet.2012.09.116

Reference yield:

: 108-88-3,15644-74-3,16713-13-6
toluene

: 1414888-81-5
C₃₇H₂₉N₂O₂⁽¹⁺⁾*Cl^(1-)

Guidance literature:: Multi-step reaction with 4 steps

1.1: aluminum (III) chloride / 20 °C / Inert atmosphere

2.1: sodium hydrogen sulfate; sodium bromate / ethyl acetate; water / 55 °C / Inert atmosphere

3.1: potassium carbonate; tetraethylammonium bromide / acetonitrile / 48 h / Reflux; Inert atmosphere

4.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 2 h / Inert atmosphere

4.2: 24 h / 125 °C / Inert atmosphere

With hydrogenchloride; aluminum (III) chloride; sodium bromate; sodium hydrogen sulfate; tetraethylammonium bromide; potassium carbonate; In 1,4-dioxane; dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1016/j.tetlet.2012.09.116 DOI:10.1016/j.tetlet.2012.09.116

Reference yield:

: 99-63-8
benzene-1,3-dicarbonyl dichloride

: 1414888-81-5
C₃₇H₂₉N₂O₂⁽¹⁺⁾*Cl^(1-)

Guidance literature:: Multi-step reaction with 4 steps

1.1: aluminum (III) chloride / 20 °C / Inert atmosphere

2.1: sodium hydrogen sulfate; sodium bromate / ethyl acetate; water / 55 °C / Inert atmosphere

3.1: potassium carbonate; tetraethylammonium bromide / acetonitrile / 48 h / Reflux; Inert atmosphere

4.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 2 h / Inert atmosphere

4.2: 24 h / 125 °C / Inert atmosphere

With hydrogenchloride; aluminum (III) chloride; sodium bromate; sodium hydrogen sulfate; tetraethylammonium bromide; potassium carbonate; In 1,4-dioxane; dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1016/j.tetlet.2012.09.116 DOI:10.1016/j.tetlet.2012.09.116