C₂₈H₄₇NO₆

Base Information

• Chemical Name: C₂₈H₄₇NO₆
• CAS No.: 1004311-48-1
• Molecular Formula: C₂₈H₄₇NO₆
• Molecular Weight: 493.684
• Mol file: 1004311-48-1.mol

Synonyms:C₂₈H₄₇NO₆

Chemical Property of C₂₈H₄₇NO₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₈H₄₇NO₆

There total 10 articles about C₂₈H₄₇NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

C28H45NO4 (1004311-47-0) → C28H47NO6 (1004311-48-1)

Guidance literature:

With osmium(VIII) oxide; methanesulfonamide; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium carbonate; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; at 0 ℃; for 24h;

DOI:10.1055/s-2007-991056

Reference yield:

1,2-epoxytetradecane (3234-28-4) → C28H47NO6 (1004311-48-1)

Guidance literature:

Multi-step reaction with 10 steps

1.1: 41 percent / H₂O / (R,R)-Co(III)(salen)*OAc / 24 h / 0 °C

2.1: 94 percent / CuI / tetrahydrofuran / 12 h / -78 °C

3.1: Et₃N / CH₂Cl₂ / 2 h

4.1: NaN₃ / dimethylformamide / 45 °C

5.1: PPh₃ / tetrahydrofuran; H₂O / 12 h / 20 °C

6.1: Na₂CO₃ / dioxane; H₂O / 0 - 20 °C

7.1: BH₃*SMe₂ / tetrahydrofuran / 3 h / 0 - 20 °C

7.2: 87 percent / NaOH; H₂O₂ / 6 h / 0 - 20 °C

8.1: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 1 h / -78 - -60 °C

9.1: tetrahydrofuran / 24 h / 20 °C

10.1: 97 percent / (DHQD)2PHAL; osmium tetroxide; MeSO₂NH₂ / K₂CO₃; potassium ferricyanide / 2-methyl-propan-2-ol; H₂O / 24 h / 0 °C

With copper(l) iodide; osmium(VIII) oxide; sodium azide; oxalyl dichloride; methanesulfonamide; dimethylsulfide borane complex; water; sodium carbonate; dimethyl sulfoxide; 1,4-bis(9-O-dihydroquinidine)phthalazine; triethylamine; triphenylphosphine; potassium carbonate; potassium hexacyanoferrate(III); In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1.1: Jacobsen's hydrolytic kinetic resolution / 5.1: Staudinger reaction / 8.1: Swern oxidation / 9.1: Wittig reaction / 10.1: Sharpless asymmetric dihydroxylation;

DOI:10.1055/s-2007-991056

Reference yield:

C16H31N3 (1004311-44-7) → C28H47NO6 (1004311-48-1)

Guidance literature:

Multi-step reaction with 6 steps

1.1: PPh₃ / tetrahydrofuran; H₂O / 12 h / 20 °C

2.1: Na₂CO₃ / dioxane; H₂O / 0 - 20 °C

3.1: BH₃*SMe₂ / tetrahydrofuran / 3 h / 0 - 20 °C

3.2: 87 percent / NaOH; H₂O₂ / 6 h / 0 - 20 °C

4.1: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 1 h / -78 - -60 °C

5.1: tetrahydrofuran / 24 h / 20 °C

6.1: 97 percent / (DHQD)2PHAL; osmium tetroxide; MeSO₂NH₂ / K₂CO₃; potassium ferricyanide / 2-methyl-propan-2-ol; H₂O / 24 h / 0 °C

With osmium(VIII) oxide; oxalyl dichloride; methanesulfonamide; dimethylsulfide borane complex; sodium carbonate; dimethyl sulfoxide; 1,4-bis(9-O-dihydroquinidine)phthalazine; triethylamine; triphenylphosphine; potassium carbonate; potassium hexacyanoferrate(III); In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; tert-butyl alcohol; 1.1: Staudinger reaction / 4.1: Swern oxidation / 5.1: Wittig reaction / 6.1: Sharpless asymmetric dihydroxylation;

DOI:10.1055/s-2007-991056

upstream raw materials:

C₂₈H₄₅NO₄

1,2-epoxytetradecane

(R)-hexadec-1-en-4-ol

C₁₆H₃₁N₃

Downstream raw materials:

C₃₅H₅₃NSO₈

Refernces