(3-(3-((6-phenylhexyloxy)carbonyl)-1H-pyrrol-1-yl)phenoxycarbonyl)cyclohexylamine

Base Information

Chemical Name:(3-(3-((6-phenylhexyloxy)carbonyl)-1H-pyrrol-1-yl)phenoxycarbonyl)cyclohexylamine
CAS No.:1392287-63-6
Molecular Formula:C₃₀H₃₆N₂O₄
Molecular Weight:488.627
Hs Code.:

Synonyms:(3-(3-((6-phenylhexyloxy)carbonyl)-1H-pyrrol-1-yl)phenoxycarbonyl)cyclohexylamine

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Chemical Property of (3-(3-((6-phenylhexyloxy)carbonyl)-1H-pyrrol-1-yl)phenoxycarbonyl)cyclohexylamine

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Technology Process of (3-(3-((6-phenylhexyloxy)carbonyl)-1H-pyrrol-1-yl)phenoxycarbonyl)cyclohexylamine

There total 2 articles about (3-(3-((6-phenylhexyloxy)carbonyl)-1H-pyrrol-1-yl)phenoxycarbonyl)cyclohexylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1245740-28-6
6-phenylhexyl-1-(3-hydroxyphenyl)-1H-pyrrole-3-carboxylate

: 3173-53-3
Cyclohexyl isocyanate

: 1392287-63-6
(3-(3-((6-phenylhexyloxy)carbonyl)-1H-pyrrol-1-yl)phenoxycarbonyl)cyclohexylamine

Guidance literature:: With triethylamine; In tetrahydrofuran; at 25 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jm300689c

Reference yield:

: 591-27-5
m-Hydroxyaniline

: 1392287-63-6
(3-(3-((6-phenylhexyloxy)carbonyl)-1H-pyrrol-1-yl)phenoxycarbonyl)cyclohexylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / water / 0.25 h / 100 °C / Inert atmosphere

2.1: silver nitrate; sodium hydroxide / methanol / 1 h / Inert atmosphere; Reflux

2.2: pH 1 / Inert atmosphere

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 48 h / 0 - 25 °C / Inert atmosphere

4.1: triethylamine / tetrahydrofuran / 16 h / 25 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; silver nitrate; acetic acid; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1021/jm300689c