Technology Process of C52H65N3O2Si
There total 6 articles about C52H65N3O2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
1,2-dimethoxyethane;
for 15h;
Heating;
DOI:10.1021/ol070245h
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / cooling
1.2: triisopropyl borate / tetrahydrofuran; hexane / 3 h / 20 °C
1.3: 70 percent / aq. HCl / tetrahydrofuran; hexane / 1 h / 20 °C
2.1: 83 percent / sodium carbonate / tetrakis(triphenylphosphine)palladium(0) / 1,2-dimethoxy-ethane / 15 h / Heating
With
n-butyllithium; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; 1,2-dimethoxyethane; hexane;
2.1: Suzuki-Miyaura coupling;
DOI:10.1021/ol070245h
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 76 percent / 18-crown-6; potassium carbonate / acetone / 48 h / Heating
2.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / cooling
2.2: triisopropyl borate / tetrahydrofuran; hexane / 3 h / 20 °C
2.3: 70 percent / aq. HCl / tetrahydrofuran; hexane / 1 h / 20 °C
3.1: 83 percent / sodium carbonate / tetrakis(triphenylphosphine)palladium(0) / 1,2-dimethoxy-ethane / 15 h / Heating
With
n-butyllithium; 18-crown-6 ether; sodium carbonate; potassium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; 1,2-dimethoxyethane; hexane; acetone;
3.1: Suzuki-Miyaura coupling;
DOI:10.1021/ol070245h
