C₄₇H₅₂ClN₇O₅

Base Information

Chemical Name:C₄₇H₅₂ClN₇O₅
CAS No.:1369595-90-3
Molecular Formula:C₄₇H₅₂ClN₇O₅
Molecular Weight:830.427
Hs Code.:

C<sub>47</sub>H<sub>52</sub>ClN<sub>7</sub>O<sub>5</sub>

Synonyms:C₄₇H₅₂ClN₇O₅

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Chemical Property of C₄₇H₅₂ClN₇O₅

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Technology Process of C₄₇H₅₂ClN₇O₅

There total 10 articles about C₄₇H₅₂ClN₇O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1007882-59-8
(S)-2-(4-bromo-1H-imidazol-2-yl)pyrrolidine-1-carboxylic acid tert-butyl ester

: 1369595-87-8
C₃₅H₄₀B₂ClNO₅

: 1369595-90-3
C₄₇H₅₂ClN₇O₅

Guidance literature:: With potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; at 90 ℃; for 15h; Inert atmosphere;

Reference yield:

: 30186-18-6
4'-bromo-2'-hydroxyacetophenone

: 1369595-90-3
C₄₇H₅₂ClN₇O₅

Guidance literature:: Multi-step reaction with 6 steps

1: acetic acid / ethanol / 6 h / Reflux

2: polyphosphoric acid / 2 h / 80 °C

3: N-chloro-succinimide / tetrahydrofuran; dichloromethane / 2.67 h / 0 - 20 °C

4: p-toluenesulfonyl chloride / toluene / 12 h / 170 °C / Microwave irradiation

5: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 2 h / 90 °C / Inert atmosphere

6: potassium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 15 h / 90 °C / Inert atmosphere

With N-chloro-succinimide; potassium acetate; potassium carbonate; acetic acid; p-toluenesulfonyl chloride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; toluene;

Reference yield:

: 69610-40-8
N-(tert-butoxycarbonyl)-L-prolinol

: 1369595-90-3
C₄₇H₅₂ClN₇O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.5 h / Cooling with ice

2.1: ammonia / methanol / 0.5 h / 20 - 30 °C

2.2: 16 h / 20 - 60 °C

3.1: N-Bromosuccinimide / dichloromethane / 1.25 h / Cooling with ice

4.1: potassium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 15 h / 90 °C / Inert atmosphere

With N-Bromosuccinimide; oxalyl dichloride; ammonia; potassium carbonate; dimethyl sulfoxide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; methanol; dichloromethane;