1-phenyl-2,2,2-trifluoro-1-<4-(1-triphenylmethyl)imidazole>ethyl phenyl thionocarbonate

Base Information

Chemical Name:1-phenyl-2,2,2-trifluoro-1-<4-(1-triphenylmethyl)imidazole>ethyl phenyl thionocarbonate
CAS No.:161530-08-1
Molecular Formula:C₃₇H₂₇F₃N₂O₂S
Molecular Weight:620.695
Hs Code.:

Synonyms:1-phenyl-2,2,2-trifluoro-1-<4-(1-triphenylmethyl)imidazole>ethyl phenyl thionocarbonate

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Chemical Property of 1-phenyl-2,2,2-trifluoro-1-<4-(1-triphenylmethyl)imidazole>ethyl phenyl thionocarbonate

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Technology Process of 1-phenyl-2,2,2-trifluoro-1-<4-(1-triphenylmethyl)imidazole>ethyl phenyl thionocarbonate

There total 3 articles about 1-phenyl-2,2,2-trifluoro-1-<4-(1-triphenylmethyl)imidazole>ethyl phenyl thionocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 161530-05-8
4-<(1-hydroxy-1-phenyl-2,2,2-trifluoro)ethyl>-N-triphenylmethylimidazole

: 1005-56-7
phenylcarbonochloridothioate

: 161530-08-1
1-phenyl-2,2,2-trifluoro-1-<4-(1-triphenylmethyl)imidazole>ethyl phenyl thionocarbonate

Guidance literature:: With dmap; In dichloromethane; for 16h; Ambient temperature;
DOI:10.3987/COM-94-S(B)77

Reference yield:

: 434-45-7
2,2,2-Trifluoroacetophenone

: 161530-08-1
1-phenyl-2,2,2-trifluoro-1-<4-(1-triphenylmethyl)imidazole>ethyl phenyl thionocarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) EtMgBr / 1.) ether, CH₂Cl₂, RT, 30 min, 2.) ether, CH₂Cl₂, 16 h

2: 51 percent / DMAP / CH₂Cl₂ / 16 h / Ambient temperature

With dmap; ethylmagnesium bromide; In dichloromethane;
DOI:10.3987/COM-94-S(B)77

Reference yield:

: 96797-15-8
N-trityl-4⁽⁵⁾-iodoimidazole

: 161530-08-1
1-phenyl-2,2,2-trifluoro-1-<4-(1-triphenylmethyl)imidazole>ethyl phenyl thionocarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) EtMgBr / 1.) ether, CH₂Cl₂, RT, 30 min, 2.) ether, CH₂Cl₂, 16 h

2: 51 percent / DMAP / CH₂Cl₂ / 16 h / Ambient temperature

With dmap; ethylmagnesium bromide; In dichloromethane;
DOI:10.3987/COM-94-S(B)77