C₂₀H₂₂O₆

Base Information

Chemical Name:C₂₀H₂₂O₆
CAS No.:1238390-52-7
Molecular Formula:C₂₀H₂₂O₆
Molecular Weight:358.391
Hs Code.:

C<sub>20</sub>H<sub>22</sub>O<sub>6</sub>

Synonyms:C₂₀H₂₂O₆

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Chemical Property of C₂₀H₂₂O₆

Chemical Property:

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Technology Process of C₂₀H₂₂O₆

There total 4 articles about C₂₀H₂₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 869852-51-7
C₁₄H₁₈O₆

: 107-19-7
propargyl alcohol

: 1238390-52-7
C₂₀H₂₂O₆

Guidance literature:: C₁₄H₁₈O₆; propargyl alcohol; With dmap; In dichloromethane; N,N-dimethyl-formamide; for 1h; Cooling with ice; Inert atmosphere;

With dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 12h; Cooling with ice; Inert atmosphere;
DOI:10.1002/pola.24108

Reference yield:

: 618-83-7
5-Hydroxyisophthalic acid

: 1238390-52-7
C₂₀H₂₂O₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / 12 h / Reflux

2.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 48 h / 90 °C

3.1: potassium hydroxide / methanol / 12 h / 50 °C

4.1: dmap / dichloromethane; N,N-dimethyl-formamide / 1 h / Cooling with ice; Inert atmosphere

4.2: 12 h / 20 °C / Cooling with ice; Inert atmosphere

With dmap; sulfuric acid; potassium carbonate; potassium iodide; potassium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/pola.24108

Reference yield:

: 197232-43-2
C₁₆H₂₂O₆

: 1238390-52-7
C₂₀H₂₂O₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / methanol / 12 h / 50 °C

2.1: dmap / dichloromethane; N,N-dimethyl-formamide / 1 h / Cooling with ice; Inert atmosphere

2.2: 12 h / 20 °C / Cooling with ice; Inert atmosphere

With dmap; potassium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/pola.24108