[Ir(Se₂)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ir(Se₂)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]B(C₆H₅)4

Base Information

• Chemical Name: [Ir(Se₂)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ir(Se₂)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]B(C₆H₅)4
• CAS No.: 82522-45-0
• Molecular Formula: C₂₄H₂₀B*C₅₂H₄₈IrP₄Se₂
• Molecular Weight: 1466.22

Synonyms:[Ir(Se₂)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ir(Se₂)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]B(C₆H₅)4

Chemical Property of [Ir(Se₂)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ir(Se₂)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]B(C₆H₅)4

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Technology Process of [Ir(Se₂)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ir(Se₂)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]B(C₆H₅)4

There total 2 articles about [Ir(Se₂)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ir(Se₂)((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2]B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(1,2-bis(diphenylphosphino)ethane)iridium(I) chloride (15390-38-2,15131-25-6) → [Ir(Se2)((C6H5)2PCH2CH2P(C6H5)2)2](1+)*B(C6H5)4(1-)=[Ir(Se2)((C6H5)2PCH2CH2P(C6H5)2)2]B(C6H5)4 (82522-45-0)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane

2: acetonitrile

In dichloromethane; acetonitrile;

DOI:10.1021/ic00140a016

Reference yield:

{Ir(Se2)(((C6H5)2PCH2)2)2}(1+)*Cl(1-)={Ir(Se2)(((C6H5)2PCH2)2)2}Cl (40603-51-8) + sodium tetraphenyl borate (143-66-8) → [Ir(Se2)((C6H5)2PCH2CH2P(C6H5)2)2](1+)*B(C6H5)4(1-)=[Ir(Se2)((C6H5)2PCH2CH2P(C6H5)2)2]B(C6H5)4 (82522-45-0)

Guidance literature:

In acetonitrile; byproducts: NaCl; (N2 or Ar); extd. (H2O);

DOI:10.1021/ic00140a016

Reference yield: 94.0%

tris(triphenylphosphine)platinum(0) (13517-35-6) + [Ir(Se2)((C6H5)2PCH2CH2P(C6H5)2)2](1+)*B(C6H5)4(1-)=[Ir(Se2)((C6H5)2PCH2CH2P(C6H5)2)2]B(C6H5)4 (82522-45-0) → [(PtSe(P(C6H5)3)2)2]*2C4H8O (74472-62-1)

Guidance literature:

With C₄H₈O; In tetrahydrofuran; acetonitrile; (N2 or Ar); Pt complex soln. added to stirred Ir complex soln., reactedfor 5 min; ppt. collected, washed with MeCN/THF, then with MeCN, dried at 55°C (vac.); elem. anal.;

DOI:10.1021/ic00140a016

upstream raw materials:

{Ir(Se₂)(((C₆H₅)2PCH₂)2)2}⁽¹⁺⁾*Cl^(1-)={Ir(Se₂)(((C₆H₅)2PCH₂)2)2}Cl

sodium tetraphenyl borate

bis(1,2-bis(diphenylphosphino)ethane)iridium(I) chloride

Downstream raw materials:

[(PtSe(P(C₆H₅)3)2)2]*2C₄H₈O

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