2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)ketone

Base Information

Chemical Name:2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)ketone
CAS No.:125335-95-7
Molecular Formula:C₂₅H₂₄N₄O₅S
Molecular Weight:492.555
Hs Code.:

Synonyms:2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)ketone

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Chemical Property of 2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)ketone

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Technology Process of 2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)ketone

There total 16 articles about 2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 148729-71-9
2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)methanol

: 125335-95-7
2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)ketone

Guidance literature:: With manganese(IV) oxide; water; In dichloromethane; for 1.5h; Heating;
DOI:10.1016/S0040-4020(01)80387-2

Reference yield: 85.0%

: 148729-71-9
2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)methanol

: (1-benzenesulfonyl 5-aza 2-indolyl)-(3-dimethylaminocarbonyl 2-methoxy pyridin-4-yl)ketone

: 125335-95-7
2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)ketone

Guidance literature:: With manganese dioxide; In dichloromethane;

Reference yield:

: 1074-98-2
3-methyl-4-nitropyridine N-oxide

: 125335-95-7
2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)ketone

Guidance literature:: Multi-step reaction with 6 steps

1: 81 percent / PCl₃ / 3.5 h / T < 0 deg C

2: 63 percent / dimethylformamide / 1 h / 90 °C

3: 91 percent / H₂ / 10percent Pd/C / ethanol / 14.7 - 22.07 Torr / 1) 1 h, 20 deg C, 2) 3 h, 60 deg C

4: 1) NaOH, Bu₄N*HSO₄ / 1) CH₂Cl₂, 2) 1 h

5: 1) LDA, tris(dioxa-3,6-heptyl)amine, tetramethylethylenediamine / 1) THF, cyclohexane, 10 min, < -75 deg C, 2) THF, -85 deg C

6: 92 percent / MnO₂, water / CH₂Cl₂ / 1.5 h / Heating

With manganese(IV) oxide; sodium hydroxide; N,N,N,N,-tetramethylethylenediamine; Tris(3,6-dioxaheptyl)amine; water; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; lithium diisopropyl amide; phosphorus trichloride; palladium on activated charcoal; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)80387-2