5-<2-(Diethylamino)-5-phenyl-1,3-dithiol-4-ylio>hexahydro-1,3-dimethyl-2,4,6-trioxo-5-pyrimidinid

Base Information

Chemical Name:5-<2-(Diethylamino)-5-phenyl-1,3-dithiol-4-ylio>hexahydro-1,3-dimethyl-2,4,6-trioxo-5-pyrimidinid
CAS No.:100515-86-4
Molecular Formula:C₁₉H₂₁N₃O₃S₂
Molecular Weight:403.526
Hs Code.:

Synonyms:5-<2-(Diethylamino)-5-phenyl-1,3-dithiol-4-ylio>hexahydro-1,3-dimethyl-2,4,6-trioxo-5-pyrimidinid

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Chemical Property of 5-<2-(Diethylamino)-5-phenyl-1,3-dithiol-4-ylio>hexahydro-1,3-dimethyl-2,4,6-trioxo-5-pyrimidinid

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Technology Process of 5-<2-(Diethylamino)-5-phenyl-1,3-dithiol-4-ylio>hexahydro-1,3-dimethyl-2,4,6-trioxo-5-pyrimidinid

There total 3 articles about 5-<2-(Diethylamino)-5-phenyl-1,3-dithiol-4-ylio>hexahydro-1,3-dimethyl-2,4,6-trioxo-5-pyrimidinid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 769-42-6
1,3-dimethylbarbituric acid

: 106064-88-4
2-(Dimethylamino)-5-phenyl-1,3-dithiolylium-4-olat

: 100515-86-4
5-<2-(Diethylamino)-5-phenyl-1,3-dithiol-4-ylio>hexahydro-1,3-dimethyl-2,4,6-trioxo-5-pyrimidinid

Guidance literature:: With sodium acetate; In acetic anhydride; at 90 ℃; for 2.5h; further without NaOAc;

Reference yield:

: 4870-65-9,31302-84-8
2-bromophenylacetic acid

: 100515-86-4
5-<2-(Diethylamino)-5-phenyl-1,3-dithiol-4-ylio>hexahydro-1,3-dimethyl-2,4,6-trioxo-5-pyrimidinid

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / Na₂CO₃

2: 34 percent / NaOAc / acetic anhydride / 90 °C

With sodium acetate; sodium carbonate; In acetic anhydride;

Reference yield:

: 58007-82-2
DL-<(Diethylamino)thioxomethylthio>phenylessigsaeure

: 100515-86-4
5-<2-(Diethylamino)-5-phenyl-1,3-dithiol-4-ylio>hexahydro-1,3-dimethyl-2,4,6-trioxo-5-pyrimidinid

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / Ac₂O, Et₃N

2: 53 percent / NaOAc / acetic anhydride / 2.5 h / 90 °C / further without NaOAc

With sodium acetate; acetic anhydride; triethylamine; In acetic anhydride;