(E)-N,N-dimethyl-1-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)phenyl)methanamine

Base Information

Chemical Name:(E)-N,N-dimethyl-1-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)phenyl)methanamine
CAS No.:1247001-30-4
Molecular Formula:C₁₇H₂₆BNO₂
Molecular Weight:287.21
Hs Code.:

Synonyms:(E)-N,N-dimethyl-1-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)phenyl)methanamine

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Chemical Property of (E)-N,N-dimethyl-1-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)phenyl)methanamine

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Technology Process of (E)-N,N-dimethyl-1-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)phenyl)methanamine

There total 3 articles about (E)-N,N-dimethyl-1-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)phenyl)methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 6274-57-3
(4-bromobenzyl)dimethylamine

: 75927-49-0
pinacol vinylboronate

: 1247001-30-4
(E)-N,N-dimethyl-1-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)phenyl)methanamine

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine; tri tert-butylphosphoniumtetrafluoroborate; In toluene; at 95 ℃; for 3h; Inert atmosphere;
DOI:10.1039/C6NJ03984G

Reference yield: 68.0%

: 1247001-32-6
N,N-dimethyl-1-(4-acetylenylphenyl)methylamine

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1247001-30-4
(E)-N,N-dimethyl-1-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)phenyl)methanamine

Guidance literature:: RuHCl(PPh₃)3; In toluene; at 50 ℃; for 12h; Inert atmosphere;

Reference yield:

: 63697-96-1
4-Ethynylbenzaldehyde

: 1247001-30-4
(E)-N,N-dimethyl-1-(4-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)vinyl)phenyl)methanamine

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 2.5 h / 20 °C / Inert atmosphere

2: (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II) / toluene / 12 h / 50 °C / Inert atmosphere

With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; toluene;
DOI:10.1021/jm500537u