C₂₃H₃₈O₃S₂

Base Information

Chemical Name:C₂₃H₃₈O₃S₂
CAS No.:954113-58-7
Molecular Formula:C₂₃H₃₈O₃S₂
Molecular Weight:426.685
Hs Code.:

C<sub>23</sub>H<sub>38</sub>O<sub>3</sub>S<sub>2</sub>

Synonyms:C₂₃H₃₈O₃S₂

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Chemical Property of C₂₃H₃₈O₃S₂

Chemical Property:

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Technology Process of C₂₃H₃₈O₃S₂

There total 8 articles about C₂₃H₃₈O₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 954113-57-6
C₁₉H₃₂OS₂

: 54882-04-1
ethyl 2-(phenylsulfinyl)acetate

: 954113-58-7
C₂₃H₃₈O₃S₂

Guidance literature:: With piperidine; In acetonitrile; at 20 ℃;
DOI:10.1016/j.tet.2007.07.090

Reference yield:

: 908370-03-6
5-[5-(tert-butyl-dimethyl-silanyloxy)-pentane-1-sulfonyl]-1-phenyl-1H-tetrazole

: 954113-58-7
C₂₃H₃₈O₃S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 74 percent / NaHMDS / tetrahydrofuran / 0.5 h / -78 °C

2.1: 96 percent / TBAF / tetrahydrofuran / 1 h / 20 °C

3.1: 85 percent / I₂; PPh₃; imidazole / diethyl ether; acetonitrile / 0.5 h / 0 °C

4.1: n-BuLi / hexane; tetrahydrofuran / 4 h / -25 °C

4.2: 70 percent / HMPA / tetrahydrofuran; hexane / 15 h / 0 °C

5.1: 89 percent / SO₃*Py; NEt₃ / dimethylsulfoxide; CH₂Cl₂ / 0.5 h / 0 °C

6.1: 63 percent / piperidine / acetonitrile / 20 °C

With piperidine; 1H-imidazole; n-butyllithium; pyridine-SO₃ complex; tetrabutyl ammonium fluoride; iodine; sodium hexamethyldisilazane; triethylamine; triphenylphosphine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; dimethyl sulfoxide; acetonitrile; 1.1: Julia coupling;
DOI:10.1016/j.tet.2007.07.090

Reference yield:

: 954113-53-2
C₁₈H₃₀N₄OSiS

: 954113-58-7
C₂₃H₃₈O₃S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: 91 percent / m-CPBA; NaHCO₃ / CH₂Cl₂ / 24 h / 20 °C

2.1: 74 percent / NaHMDS / tetrahydrofuran / 0.5 h / -78 °C

3.1: 96 percent / TBAF / tetrahydrofuran / 1 h / 20 °C

4.1: 85 percent / I₂; PPh₃; imidazole / diethyl ether; acetonitrile / 0.5 h / 0 °C

5.1: n-BuLi / hexane; tetrahydrofuran / 4 h / -25 °C

5.2: 70 percent / HMPA / tetrahydrofuran; hexane / 15 h / 0 °C

6.1: 89 percent / SO₃*Py; NEt₃ / dimethylsulfoxide; CH₂Cl₂ / 0.5 h / 0 °C

7.1: 63 percent / piperidine / acetonitrile / 20 °C

With piperidine; 1H-imidazole; n-butyllithium; pyridine-SO₃ complex; tetrabutyl ammonium fluoride; iodine; sodium hexamethyldisilazane; sodium hydrogencarbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; dimethyl sulfoxide; acetonitrile; 2.1: Julia coupling;
DOI:10.1016/j.tet.2007.07.090