6-(6-bromo-7-nitro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N-phenylhexanamide

Base Information

Chemical Name:6-(6-bromo-7-nitro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N-phenylhexanamide
CAS No.:1334715-87-5
Molecular Formula:C₂₄H₂₀BrN₃O₅
Molecular Weight:510.344
Hs Code.:

Synonyms:6-(6-bromo-7-nitro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N-phenylhexanamide

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Chemical Property of 6-(6-bromo-7-nitro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N-phenylhexanamide

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Technology Process of 6-(6-bromo-7-nitro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N-phenylhexanamide

There total 4 articles about 6-(6-bromo-7-nitro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N-phenylhexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 27742-73-0
4-bromo-5-nitro-1,8-naphthalene dicarboxylic acid anhydride

: 115012-25-4
6-aminohexanoic acid phenylamide

: 1334715-87-5
6-(6-bromo-7-nitro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N-phenylhexanamide

Guidance literature:: In ethanol; for 0.666667h; Reflux;
DOI:10.1002/anie.201101317

Reference yield:

: 6404-29-1
6-(tert-butoxycarbonylamino)hexanoic acid

: 1334715-87-5
6-(6-bromo-7-nitro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N-phenylhexanamide

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine; HATU / tetrahydrofuran / 20 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 0.75 h / 20 °C

3: ethanol / 0.67 h / Reflux

With N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1002/anie.201101317

Reference yield:

: 329967-27-3
6-(tert-butyloxycarbonylamino)-N-phenyl-hexanamide

: 1334715-87-5
6-(6-bromo-7-nitro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N-phenylhexanamide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 0.75 h / 20 °C

2: ethanol / 0.67 h / Reflux

With trifluoroacetic acid; In ethanol; dichloromethane;
DOI:10.1002/anie.201101317