(S₂,R₃,R_S)-2-tert-butyl-2-hydroxy-3-<(4-methylphenyl)sulfinyl>butanenitrile

Base Information

Chemical Name:(S₂,R₃,R_S)-2-tert-butyl-2-hydroxy-3-<(4-methylphenyl)sulfinyl>butanenitrile
CAS No.:144694-79-1
Molecular Formula:C₁₅H₂₁NO₂S
Molecular Weight:279.403
Hs Code.:

(S<sub>2</sub>,R<sub>3</sub>,R<sub>S</sub>)-2-tert-butyl-2-hydroxy-3-<(4-methylphenyl)sulfinyl>butanenitrile

Synonyms:(S₂,R₃,R_S)-2-tert-butyl-2-hydroxy-3-<(4-methylphenyl)sulfinyl>butanenitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S₂,R₃,R_S)-2-tert-butyl-2-hydroxy-3-<(4-methylphenyl)sulfinyl>butanenitrile

Chemical Property:

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Technology Process of (S₂,R₃,R_S)-2-tert-butyl-2-hydroxy-3-<(4-methylphenyl)sulfinyl>butanenitrile

There total 5 articles about (S₂,R₃,R_S)-2-tert-butyl-2-hydroxy-3-<(4-methylphenyl)sulfinyl>butanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3938-95-2
2,2-dimethyl-propanoic acid ethyl ester

: 144694-79-1
(S₂,R₃,R_S)-2-tert-butyl-2-hydroxy-3-<(4-methylphenyl)sulfinyl>butanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 1) LDA / 1) THF, 0 deg C, 30 min, 2) -78 deg C, THF, 2 h

2: toluene / 2 h / 0 °C

With lithium diisopropyl amide; In toluene;
DOI:10.1021/jo00052a044

Reference yield:

: 1519-40-0
(+)-(R)-ethyl p-tolyl sulfoxide

: 144694-79-1
(S₂,R₃,R_S)-2-tert-butyl-2-hydroxy-3-<(4-methylphenyl)sulfinyl>butanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 1) LDA / 1) THF, 0 deg C, 30 min, 2) -78 deg C, THF, 2 h

2: toluene / 2 h / 0 °C

With lithium diisopropyl amide; In toluene;
DOI:10.1021/jo00052a044

Reference yield:

: 1519-40-0
(+)-(R)-ethyl p-tolyl sulfoxide

: 144694-79-1,144786-51-6,144786-52-7
(R₂,R₃,R_S)-2-tert-butyl-2-hydroxy-3-<(4-methylphenyl)sulfinyl>butanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 1) LDA / 1) THF, 0 deg C, 30 min, 2) -78 deg C, THF, 2 h

2: ZnBr₂ / toluene; tetrahydrofuran / 2 h / Ambient temperature

With zinc dibromide; lithium diisopropyl amide; In tetrahydrofuran; toluene;
DOI:10.1021/jo00052a044