Benzyl-2-azido-2-desoxy-4,6-O-isopropyliden-3-O-<(R)-1-(methoxycarbonyl)ethyl>-α-D-glucopyranosyd

Base Information

Chemical Name:Benzyl-2-azido-2-desoxy-4,6-O-isopropyliden-3-O-<(R)-1-(methoxycarbonyl)ethyl>-α-D-glucopyranosyd
CAS No.:106567-78-6
Molecular Formula:C₂₀H₂₇N₃O₇
Molecular Weight:421.45
Hs Code.:

Synonyms:Benzyl-2-azido-2-desoxy-4,6-O-isopropyliden-3-O-<(R)-1-(methoxycarbonyl)ethyl>-α-D-glucopyranosyd

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Chemical Property of Benzyl-2-azido-2-desoxy-4,6-O-isopropyliden-3-O-<(R)-1-(methoxycarbonyl)ethyl>-α-D-glucopyranosyd

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Technology Process of Benzyl-2-azido-2-desoxy-4,6-O-isopropyliden-3-O-<(R)-1-(methoxycarbonyl)ethyl>-α-D-glucopyranosyd

There total 4 articles about Benzyl-2-azido-2-desoxy-4,6-O-isopropyliden-3-O-<(R)-1-(methoxycarbonyl)ethyl>-α-D-glucopyranosyd which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 106567-72-0
O-<2-Azido-2-desoxy-4,6-O-isopropyliden-3-O-<(R)-1-(methoxycarbonyl)ethyl>-α-D-glucopyranosyl>-trichloracetimidat

: 100-51-6,185532-71-2
benzyl alcohol

: 106567-78-6
Benzyl-2-azido-2-desoxy-4,6-O-isopropyliden-3-O-<(R)-1-(methoxycarbonyl)ethyl>-α-D-glucopyranosyd

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 ℃; for 4h;

Reference yield:

: 99049-68-0
tert-Butyldimethylsilyl-2-azido-2-desoxy-4,6-O-isopropyliden-β-D-glucopyranosid

: 106567-78-6
Benzyl-2-azido-2-desoxy-4,6-O-isopropyliden-3-O-<(R)-1-(methoxycarbonyl)ethyl>-α-D-glucopyranosyd

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) DME, room temp.; 2.) 3 h

2: 71 percent / silica gel, (NBu₄)F / tetrahydrofuran / 2 h / -50 °C

3: NaH / CH₂Cl₂

4: 70 percent / 0,1 N CF₃SO₃Si(CH₃)3 / CH₂Cl₂ / 4 h / -20 °C

With trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; silica gel; sodium hydride; In tetrahydrofuran; dichloromethane;

Reference yield:

: 2-Azido-2-desoxy-4,6-isopropyliden-3-O-<(R)-1-(methoxycarbonyl)ethyl>-D-glucopyranose

: 106567-78-6
Benzyl-2-azido-2-desoxy-4,6-O-isopropyliden-3-O-<(R)-1-(methoxycarbonyl)ethyl>-α-D-glucopyranosyd

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / CH₂Cl₂

2: 70 percent / 0,1 N CF₃SO₃Si(CH₃)3 / CH₂Cl₂ / 4 h / -20 °C

With trimethylsilyl trifluoromethanesulfonate; sodium hydride; In dichloromethane;