Technology Process of C41H54O6
There total 11 articles about C41H54O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium cyanoborohydride; acetic acid;
at 20 ℃;
for 1.5h;
Inert atmosphere;
DOI:10.1021/jo102054r
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
3: lithium aluminium tetrahydride / tetrahydrofuran / -10 °C / Inert atmosphere; Reflux
4: pyridine; dmap / 6 h / Inert atmosphere; Reflux
5: sodium cyanoborohydride; acetic acid / 1.5 h / 20 °C / Inert atmosphere
With
pyridine; dmap; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; sodium cyanoborohydride; acetic acid; triphenylphosphine;
In
tetrahydrofuran;
2: Mitsunobu reaction;
DOI:10.1021/jo102054r
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / -10 °C / Inert atmosphere; Reflux
2: pyridine; dmap / 6 h / Inert atmosphere; Reflux
3: sodium cyanoborohydride; acetic acid / 1.5 h / 20 °C / Inert atmosphere
With
pyridine; dmap; lithium aluminium tetrahydride; sodium cyanoborohydride; acetic acid;
In
tetrahydrofuran;
DOI:10.1021/jo102054r
