C₄₇H₄₅N₁₃O₇S₆

Base Information

Chemical Name:C₄₇H₄₅N₁₃O₇S₆
CAS No.:960061-68-1
Molecular Formula:C₄₇H₄₅N₁₃O₇S₆
Molecular Weight:1096.35
Hs Code.:

C<sub>47</sub>H<sub>45</sub>N<sub>13</sub>O<sub>7</sub>S<sub>6</sub>

Synonyms:C₄₇H₄₅N₁₃O₇S₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₇H₄₅N₁₃O₇S₆

Chemical Property:

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Technology Process of C₄₇H₄₅N₁₃O₇S₆

There total 6 articles about C₄₇H₄₅N₁₃O₇S₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: GE₂₂₇₀ A

: 960061-68-1
C₄₇H₄₅N₁₃O₇S₆

Guidance literature:: Multi-step reaction with 6 steps

1: formic acid

2: water; sodium hydroxide / tetrahydrofuran / 1.5 h / 60 °C

3: triethylamine / acetone / Sonication

4: sodium azide / acetone / 1.33 h / 60 °C

5: 14 h / 80 °C

6: trifluoroacetic acid / dichloromethane / 2 h

With formic acid; sodium azide; water; triethylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; dichloromethane; acetone; 5: Curtius rearrangement;
DOI:10.1021/jm101602q

Reference yield:

: 960061-70-5
C₅₂H₅₃N₁₃O₉S₆

: 960061-68-1
C₄₇H₄₅N₁₃O₇S₆

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 2h;
DOI:10.1021/jm101602q

Reference yield:

: 960062-64-0
C₄₈H₄₄N₁₂O₉S₆

: 960061-68-1
C₄₇H₄₅N₁₃O₇S₆

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / acetone / Sonication

2: sodium azide / acetone / 1.33 h / 60 °C

3: 14 h / 80 °C

4: trifluoroacetic acid / dichloromethane / 2 h

With sodium azide; triethylamine; trifluoroacetic acid; In dichloromethane; acetone; 3: Curtius rearrangement;
DOI:10.1021/jm101602q