Technology Process of C61H49NO16S
There total 11 articles about C61H49NO16S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trimethylsilyl trifluoromethanesulfonate;
In
dichloromethane;
at 0 - 20 ℃;
for 2h;
DOI:10.1016/j.tetlet.2011.01.149
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2-chloro-1,3-dimethyl imidazolium chloride
2: p-toluenesulfonic acid monohydrate / N,N-dimethyl-formamide; benzene / 4 h / 17 Torr / Reflux; Dean-Stark apparatus
3: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2 h / 0 - 20 °C
With
2-chloro-1,3-dimethyl imidazolium chloride; trimethylsilyl trifluoromethanesulfonate; p-toluenesulfonic acid monohydrate;
In
dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.tetlet.2011.01.149
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine
2: boron trifluoride diethyl etherate / dichloromethane
3: methanol; sodium methylate
4: p-toluenesulfonic acid monohydrate / N,N-dimethyl-formamide; benzene / 4 h / 17 Torr / Reflux; Dean-Stark apparatus
5: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2 h / 0 - 20 °C
With
pyridine; methanol; trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; p-toluenesulfonic acid monohydrate; sodium methylate;
In
dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.tetlet.2011.01.149