C₃₅H₄₈O₈Si

Base Information

Chemical Name:C₃₅H₄₈O₈Si
CAS No.:214484-10-3
Molecular Formula:C₃₅H₄₈O₈Si
Molecular Weight:624.847
Hs Code.:

C<sub>35</sub>H<sub>48</sub>O<sub>8</sub>Si

Synonyms:C₃₅H₄₈O₈Si

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Chemical Property of C₃₅H₄₈O₈Si

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Technology Process of C₃₅H₄₈O₈Si

There total 15 articles about C₃₅H₄₈O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 214484-00-1
C₁₉H₃₀O₈

: 214484-10-3
C₃₅H₄₈O₈Si

Guidance literature:: With pyridine; dmap; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1016/S0040-4020(02)00050-9

Reference yield:

: 214483-93-9
(3E,5S,9S,10E)-5,9-dimethyl-1,13-bis(benzyloxy)-3,10-tridecadien-7-one

: 214484-10-3
C₃₅H₄₈O₈Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: AD-mix-α / 2-methyl-propan-2-ol; H2O / 24 h / 0 °C

2.1: CSA / benzene; methanol / 32 h

2.2: H₂ / Pd(OH)2 / ethanol / 12 h / 20 °C / 760 Torr

3.1: 98 percent / TFA / methanol / 0.83 h / Heating

4.1: 75 percent / NMO; 4 Angstroem molecular sieves; TPAP / 2-methyl-propan-2-ol; acetonitrile / 20 °C

5.1: pyridine / tetrahydrofuran; toluene / 0.75 h / -78 - 20 °C

5.2: 9-BBN / tetrahydrofuran; toluene / 0.5 h / 20 °C

5.3: 40 percent / NaBO₃*4H₂O / tetrahydrofuran; toluene / 2 h

6.1: Dess-Martin periodinane reagent / CH₂Cl₂ / 2.5 h / 20 °C

7.1: 77 percent / TiCl₄ / CH₂Cl₂ / 0.33 h / -78 °C

8.1: 91 percent / pyridine; DMAP / 27 h / 20 °C

9.1: 99 percent / IBr / toluene; CH₂Cl₂ / 3 h / -80 °C

10.1: 90 percent / aq. LiOH / 1,2-dimethoxy-ethane / 13 h / 60 °C

11.1: 90 percent / pyridine; DMAP / CH₂Cl₂ / 16 h / 20 °C

With pyridine; dmap; lithium hydroxide; AD-mix-α; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; camphor-10-sulfonic acid; iodine(I) bromide; titanium tetrachloride; Dess-Martin periodane; trifluoroacetic acid; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; water; toluene; acetonitrile; tert-butyl alcohol; benzene;
DOI:10.1016/S0040-4020(02)00050-9

Reference yield:

: 214483-92-8
(3S,4E)-3-methyl-7-benzyloxy-4-heptenoic acid ethyl ester

: 214484-10-3
C₃₅H₄₈O₈Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: 84 percent / HMDS; TMEDA; n-BuLi / tetrahydrofuran / 0 °C

2.1: 96 percent / aq. LiCl / dimethylsulfoxide / 0.67 h / 190 °C

3.1: AD-mix-α / 2-methyl-propan-2-ol; H2O / 24 h / 0 °C

4.1: CSA / benzene; methanol / 32 h

4.2: H₂ / Pd(OH)2 / ethanol / 12 h / 20 °C / 760 Torr

5.1: 98 percent / TFA / methanol / 0.83 h / Heating

6.1: 75 percent / NMO; 4 Angstroem molecular sieves; TPAP / 2-methyl-propan-2-ol; acetonitrile / 20 °C

7.1: pyridine / tetrahydrofuran; toluene / 0.75 h / -78 - 20 °C

7.2: 9-BBN / tetrahydrofuran; toluene / 0.5 h / 20 °C

7.3: 40 percent / NaBO₃*4H₂O / tetrahydrofuran; toluene / 2 h

8.1: Dess-Martin periodinane reagent / CH₂Cl₂ / 2.5 h / 20 °C

9.1: 77 percent / TiCl₄ / CH₂Cl₂ / 0.33 h / -78 °C

10.1: 91 percent / pyridine; DMAP / 27 h / 20 °C

11.1: 99 percent / IBr / toluene; CH₂Cl₂ / 3 h / -80 °C

12.1: 90 percent / aq. LiOH / 1,2-dimethoxy-ethane / 13 h / 60 °C

13.1: 90 percent / pyridine; DMAP / CH₂Cl₂ / 16 h / 20 °C

With pyridine; dmap; lithium hydroxide; AD-mix-α; n-butyllithium; N-methyl-2-indolinone; tetrapropylammonium perruthennate; N,N,N,N,-tetramethylethylenediamine; 4 A molecular sieve; camphor-10-sulfonic acid; iodine(I) bromide; titanium tetrachloride; Dess-Martin periodane; 1,1,1,3,3,3-hexamethyl-disilazane; trifluoroacetic acid; lithium chloride; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; water; dimethyl sulfoxide; toluene; acetonitrile; tert-butyl alcohol; benzene;
DOI:10.1016/S0040-4020(02)00050-9