ethyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-(triphenylmethyl)-α-D-arabino-hexopyranoside

Base Information

Chemical Name:ethyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-(triphenylmethyl)-α-D-arabino-hexopyranoside
CAS No.:73679-59-1
Molecular Formula:C₂₉H₃₄O₃
Molecular Weight:430.587
Hs Code.:

Synonyms:ethyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-(triphenylmethyl)-α-D-arabino-hexopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-(triphenylmethyl)-α-D-arabino-hexopyranoside

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Technology Process of ethyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-(triphenylmethyl)-α-D-arabino-hexopyranoside

There total 2 articles about ethyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-(triphenylmethyl)-α-D-arabino-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73656-99-2
ethyl 2,3,4-trideoxy-2-C-methyl-4-C-methylene-6-O-triphenylmethyl-α-D-threo-hexopyranoside

: 73657-02-0
ethyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-(triphenylmethyl)-α-D-lyxo-hexopyranoside

: 73679-59-1
ethyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-(triphenylmethyl)-α-D-arabino-hexopyranoside

Guidance literature:: With hydrogen; W-8 Raney nickel; In ethyl acetate; for 120h; Yield given; Ambient temperature; other catalysts;
DOI:10.1021/jo00345a008

Reference yield:

: 66149-54-0
ethyl 2,3-dideoxy-2-C-methyl-6-O-triphenylmethyl-α-D-threo-hexopyranoside-4-ulose

: 73679-59-1
ethyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-(triphenylmethyl)-α-D-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-butyllithium / 1.) diethyl ether, room temp., 1 h, 2.) 6 h

2: H₂ / W-8 Raney nickel / ethyl acetate / Ambient temperature; other catalysts

With n-butyllithium; hydrogen; W-8 Raney nickel; In ethyl acetate;
DOI:10.1021/jo00345a008