Technology Process of C30H42N2O5
There total 3 articles about C30H42N2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
tert-butylbenzene;
at 160 ℃;
for 120h;
Inert atmosphere;
Sealed tube;
DOI:10.1021/ol1026602
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere
1.2: 2.5 h / 0 - 20 °C / Inert atmosphere
2.1: water; acetic acid / 21.5 h / 20 - 40 °C / Inert atmosphere
3.1: tert-butylbenzene / 120 h / 160 °C / Inert atmosphere; Sealed tube
With
water; sodium hydride; acetic acid;
In
tert-butylbenzene; N,N-dimethyl-formamide;
3.1: Sequential Claisen/Claisen rearrangement;
DOI:10.1021/ol1026602
- Guidance literature:
-
Multi-step reaction with 2 steps
1: water; acetic acid / 21.5 h / 20 - 40 °C / Inert atmosphere
2: tert-butylbenzene / 120 h / 160 °C / Inert atmosphere; Sealed tube
With
water; acetic acid;
In
tert-butylbenzene;
2: Sequential Claisen/Claisen rearrangement;
DOI:10.1021/ol1026602