1-O-benzyl-2-decoxy-3-O-(1',1',20',20'-²H₄-10'-undecenoxy)-rac-glycerol

Base Information

• Chemical Name: 1-O-benzyl-2-decoxy-3-O-(1',1',20',20'-²H₄-10'-undecenoxy)-rac-glycerol
• CAS No.: 1019641-37-2
• Molecular Formula: C₃₁H₅₄O₃
• Molecular Weight: 476.752
• Mol file: 1019641-37-2.mol

Synonyms:1-O-benzyl-2-decoxy-3-O-(1',1',20',20'-²H₄-10'-undecenoxy)-rac-glycerol

Chemical Property of 1-O-benzyl-2-decoxy-3-O-(1',1',20',20'-²H₄-10'-undecenoxy)-rac-glycerol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-O-benzyl-2-decoxy-3-O-(1',1',20',20'-²H₄-10'-undecenoxy)-rac-glycerol

There total 1 articles about 1-O-benzyl-2-decoxy-3-O-(1',1',20',20'-²H₄-10'-undecenoxy)-rac-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

[1',1'-2H2]-undec-10-enyl methanesulfonate (1019641-49-6) + 3-(benzyloxy)-2-(decyloxy)propan-1-ol (181173-55-7) → 1-O-benzyl-2-decoxy-3-O-(1',1',20',20'-2H4-10'-undecenoxy)-rac-glycerol (1019641-37-2)

Guidance literature:

With sodium hydride; In tetrahydrofuran; Heating;

DOI:10.1021/ja710190p

Reference yield: 81.0%

1-O-benzyl-2-decoxy-3-O-(1',1',20',20'-2H4-10'-undecenoxy)-rac-glycerol (1019641-37-2) → 1,1'-di-O-benzyl-2,2'-di-O-decyl-3,3'-di-O-(1',1',20',20'-2H4-10'-eicosenenyl)-bis-(rac-glycerol) (1019641-39-4)

Guidance literature:

Grubbs catalyst first generation; In dichloromethane; for 12h; Heating;

DOI:10.1021/ja710190p

upstream raw materials:

[1',1'-²H₂]-undec-10-enyl methanesulfonate

3-(benzyloxy)-2-(decyloxy)propan-1-ol

Downstream raw materials:

1,1'-di-O-benzyl-2,2'-di-O-decyl-3,3'-di-O-(1',1',20',20'-²H₄-10'-eicosenenyl)-bis-(rac-glycerol)