phenyl 2,3,6-tri-O-methyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-1-thio-β-D-glucopyranoside

Base Information

• Chemical Name: phenyl 2,3,6-tri-O-methyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-1-thio-β-D-glucopyranoside
• CAS No.: 895576-60-0
• Molecular Formula: C₂₄H₃₈O₁₀S
• Molecular Weight: 518.626

Synonyms:phenyl 2,3,6-tri-O-methyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-1-thio-β-D-glucopyranoside

Chemical Property of phenyl 2,3,6-tri-O-methyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-1-thio-β-D-glucopyranoside

Chemical Property:

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Technology Process of phenyl 2,3,6-tri-O-methyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-1-thio-β-D-glucopyranoside

There total 1 articles about phenyl 2,3,6-tri-O-methyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.4%

phenyl 4-O-p-methoxybenzyl-2,3,6-tri-O-methyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-1-thio-β-D-glucopyranoside (895576-59-7) → phenyl 2,3,6-tri-O-methyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-1-thio-β-D-glucopyranoside (895576-60-0)

Guidance literature:

With ammonium cerium (IV) nitrate; water; In acetonitrile; at 0 ℃; for 12h;

Reference yield: 81.0%

phenyl 2,3,6-tri-O-methyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-1-thio-β-D-glucopyranoside (895576-60-0) + 4-O-acetyl-2,3,6-tri-O-benzyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-benzyl-α-D-glucopyranosyl imidate (895576-79-1) → phenyl 4-O-acetyl-2,3,6-tri-O-benzyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-benzyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-1-thio-β-D-glucopyranoside (895576-96-2)

Guidance literature:

boron trifluoride diethyl etherate; In dichloromethane; at -78 - -50 ℃; for 26h;

Reference yield: 55.0%

4-O-acetyl-3-O-benzyl-2,6-O-pivaloyl-D-glucopyranosyl fluoride (895576-83-7) + phenyl 2,3,6-tri-O-methyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-1-thio-β-D-glucopyranoside (895576-60-0) → phenyl 4-O-acetyl-3-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-1-thio-β-D-glucopyranoside (895576-90-6)

Guidance literature:

With silver perchlorate; bis(cyclopentadienyl)hafnium dichloride; In benzene; at 20 ℃; for 3.5h;

upstream raw materials:

phenyl 4-O-p-methoxybenzyl-2,3,6-tri-O-methyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-1-thio-β-D-glucopyranoside

Downstream raw materials:

phenyl 4-O-acetyl-2,3,6-tri-O-methyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-1-thio-β-D-glucopyranoside

phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-[1-4]-2,3,6-tri-O-acetyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-1-thio-β-D-glucopyranoside

phenyl 4-O-acetyl-2,3,6-tri-O-benzyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-benzyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-1-thio-β-D-glucopyranoside

phenyl 4-O-acetyl-3-O-benzyl-2,6-di-O-pivaloyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-methyl-1-thio-β-D-glucopyranoside

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