2-butyl-4-iodo-1-<4-(2-cyanophenyl)phenyl>methyl-imidazole-5-carbox-aldehyde

Base Information

Chemical Name:2-butyl-4-iodo-1-<4-(2-cyanophenyl)phenyl>methyl-imidazole-5-carbox-aldehyde
CAS No.:154371-55-8
Molecular Formula:C₂₂H₂₀IN₃O
Molecular Weight:469.325
Hs Code.:

Synonyms:2-butyl-4-iodo-1-<4-(2-cyanophenyl)phenyl>methyl-imidazole-5-carbox-aldehyde

Suppliers and Price of 2-butyl-4-iodo-1-<4-(2-cyanophenyl)phenyl>methyl-imidazole-5-carbox-aldehyde

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Chemical Property of 2-butyl-4-iodo-1-<4-(2-cyanophenyl)phenyl>methyl-imidazole-5-carbox-aldehyde

Chemical Property:

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Technology Process of 2-butyl-4-iodo-1-<4-(2-cyanophenyl)phenyl>methyl-imidazole-5-carbox-aldehyde

There total 4 articles about 2-butyl-4-iodo-1-<4-(2-cyanophenyl)phenyl>methyl-imidazole-5-carbox-aldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50790-93-7
2-butyl-1H-imidazole

: 154371-55-8
2-butyl-4-iodo-1-<4-(2-cyanophenyl)phenyl>methyl-imidazole-5-carbox-aldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / iodine, Na₂CO₃ / dioxane; H₂O / 23 h / Ambient temperature

2: 99 percent / K₂CO₃ / dimethylformamide / 19 h

3: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 25 min, 2.) THF, hexane, 30 min

4: 98 percent / conc. HCl / aq. ethanol / 1.25 h / Heating

5: 70 percent / K₂CO₃ / dimethylformamide / 60 h

With hydrogenchloride; n-butyllithium; iodine; sodium carbonate; potassium carbonate; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1080/00397919308011184

Reference yield:

: 154371-61-6
2-butyl-4,5-diiodoimidazole

: 154371-55-8
2-butyl-4-iodo-1-<4-(2-cyanophenyl)phenyl>methyl-imidazole-5-carbox-aldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / K₂CO₃ / dimethylformamide / 19 h

2: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 25 min, 2.) THF, hexane, 30 min

3: 98 percent / conc. HCl / aq. ethanol / 1.25 h / Heating

4: 70 percent / K₂CO₃ / dimethylformamide / 60 h

With hydrogenchloride; n-butyllithium; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1080/00397919308011184

Reference yield:

: 154371-62-7
1-(benzyloxymethyl)-2-butyl-4,5-diiodoimidazole

: 154371-55-8
2-butyl-4-iodo-1-<4-(2-cyanophenyl)phenyl>methyl-imidazole-5-carbox-aldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 25 min, 2.) THF, hexane, 30 min

2: 98 percent / conc. HCl / aq. ethanol / 1.25 h / Heating

3: 70 percent / K₂CO₃ / dimethylformamide / 60 h

With hydrogenchloride; n-butyllithium; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1080/00397919308011184