Colletochlorin D

Base Information

Chemical Name:Colletochlorin D
CAS No.:53939-17-6
Molecular Formula:C₁₃H₁₅ClO₃
Molecular Weight:254.713
Hs Code.:
UNII:0K753AQ919
Nikkaji Number:J10.817K
Wikidata:Q27896912
Mol file:53939-17-6.mol

Synonyms:Colletochlorin D;Colletochlorin-d;0K753AQ919;UNII-0K753AQ919;53939-17-6;3-Chloro-4,6-dihydroxy-2-methyl-5-(3-methyl-2-buten-1-yl)benzaldehyde;Benzaldehyde, 3-chloro-4,6-dihydroxy-2-methyl-5-(3-methyl-2-butenyl)-;Benzaldehyde, 3-chloro-4,6-dihydroxy-2-methyl-5-(3-methyl-2-buten-1-yl)-;Q27896912

Suppliers and Price of Colletochlorin D

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of Colletochlorin D

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:254.0709720
Heavy Atom Count:17
Complexity:299

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=C(C(=C1Cl)O)CC=C(C)C)O)C=O

Technology Process of Colletochlorin D

There total 13 articles about Colletochlorin D which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 81477-09-0
3-chloro-4,6-dimethoxy-2-methyl-5-(3-methyl-2-butenyl)benzaldehyde

: 53939-17-6
5-chloro-2,4-dihydroxy-6-methyl-3-(3-methyl-2-butenyl)benzaldehyde

Guidance literature:: With bromomagnesium ethanethiolate; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)84050-2

Reference yield: 42.0%

: 83324-59-8
3-chloro-4,6-dihydroxy-2-methyl-benzaldehyde

: 870-63-3
prenyl bromide

: 53939-17-6
5-chloro-2,4-dihydroxy-6-methyl-3-(3-methyl-2-butenyl)benzaldehyde

Guidance literature:: With aluminum oxide; barium(II) oxide; In diethyl ether; hexane; for 96h;
DOI:10.1021/jo00373a030

Reference yield:

: 487-69-4
2,4-dihydroxy-6-methylbenzaldehyde

: 53939-17-6
5-chloro-2,4-dihydroxy-6-methyl-3-(3-methyl-2-butenyl)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / SO₂Cl₂ / diethyl ether / 0 - 20 °C

2: 25 percent / 10percent aq. KOH / 0.67 h

With potassium hydroxide; sulfuryl dichloride; In diethyl ether;
DOI:10.1021/jo00221a009