4-(4-(benzyloxy)phenyl)-7-(4,5-bis(benzyloxy)-2-chlorophenyl)-5-(methoxymethoxy)benzo-[d][1,3]dioxol-6-yl formate

Base Information

• Chemical Name: 4-(4-(benzyloxy)phenyl)-7-(4,5-bis(benzyloxy)-2-chlorophenyl)-5-(methoxymethoxy)benzo-[d][1,3]dioxol-6-yl formate
• CAS No.: 1192737-23-7
• Molecular Formula: C₄₃H₃₅ClO₉
• Molecular Weight: 731.198

Synonyms:4-(4-(benzyloxy)phenyl)-7-(4,5-bis(benzyloxy)-2-chlorophenyl)-5-(methoxymethoxy)benzo-[d][1,3]dioxol-6-yl formate

Chemical Property of 4-(4-(benzyloxy)phenyl)-7-(4,5-bis(benzyloxy)-2-chlorophenyl)-5-(methoxymethoxy)benzo-[d][1,3]dioxol-6-yl formate

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Technology Process of 4-(4-(benzyloxy)phenyl)-7-(4,5-bis(benzyloxy)-2-chlorophenyl)-5-(methoxymethoxy)benzo-[d][1,3]dioxol-6-yl formate

There total 1 articles about 4-(4-(benzyloxy)phenyl)-7-(4,5-bis(benzyloxy)-2-chlorophenyl)-5-(methoxymethoxy)benzo-[d][1,3]dioxol-6-yl formate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

7-(4-(benzyloxy)phenyl)-4-(4,5-bis(benzyloxy)-2-chlorophenyl)-6-(methoxymethoxy)benzo-[d][1,3]dioxole-5-carbaldehyde (1192737-21-5) → 4-(4-(benzyloxy)phenyl)-7-(4,5-bis(benzyloxy)-2-chlorophenyl)-5-(methoxymethoxy)benzo-[d][1,3]dioxol-6-yl formate (1192737-23-7)

Guidance literature:

With potassium fluoride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -20 - 0 ℃; for 1.33333h; Inert atmosphere;

DOI:10.1021/ol9020833

Reference yield: 88.0%

4-(4-(benzyloxy)phenyl)-7-(4,5-bis(benzyloxy)-2-chlorophenyl)-5-(methoxymethoxy)benzo-[d][1,3]dioxol-6-yl formate (1192737-23-7) → 7,8-bis(benzyloxy)-3-(4-(benzyloxy)phenyl)-4-(methoxymethoxy)-1,2-methylenedioxydibenzofuran (1192737-25-9)

Guidance literature:

With pyridine; copper(I) oxide; at 110 ℃; for 5h; Inert atmosphere;

DOI:10.1021/ol9020833

Reference yield: 86.0%

4-(4-(benzyloxy)phenyl)-7-(4,5-bis(benzyloxy)-2-chlorophenyl)-5-(methoxymethoxy)benzo-[d][1,3]dioxol-6-yl formate (1192737-23-7) → 7-(4-(benzyloxy)phenyl)-4-(4,5-bis(benzyloxy)-2-chlorophenyl)-6-(methoxymethoxy)benzo-[d][1,3]dioxol-5-ol (1192737-24-8)

Guidance literature:

With methanol; potassium carbonate; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;

DOI:10.1021/ol9020833

upstream raw materials:

7-(4-(benzyloxy)phenyl)-4-(4,5-bis(benzyloxy)-2-chlorophenyl)-6-(methoxymethoxy)benzo-[d][1,3]dioxole-5-carbaldehyde

Downstream raw materials:

7-(4-(benzyloxy)phenyl)-4-(4,5-bis(benzyloxy)-2-chlorophenyl)-6-(methoxymethoxy)benzo-[d][1,3]dioxol-5-ol

7,8-bis(benzyloxy)-3-(4-(benzyloxy)phenyl)-4-(methoxymethoxy)-1,2-methylenedioxydibenzofuran

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