1-O-Allyloxycarbonyl-2,3,5-tri-O-benzyl-4-O-<2,4-di-O-acetyl-3-O-<2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranosyl>-D-ribitol

Base Information

Chemical Name:1-O-Allyloxycarbonyl-2,3,5-tri-O-benzyl-4-O-<2,4-di-O-acetyl-3-O-<2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranosyl>-D-ribitol
CAS No.:131328-68-2
Molecular Formula:C₆₆H₈₂O₃₀
Molecular Weight:1355.36
Hs Code.:

1-O-Allyloxycarbonyl-2,3,5-tri-O-benzyl-4-O-<2,4-di-O-acetyl-3-O-<2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranosyl>-D-ribitol

Synonyms:1-O-Allyloxycarbonyl-2,3,5-tri-O-benzyl-4-O-<2,4-di-O-acetyl-3-O-<2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranosyl>-D-ribitol

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Chemical Property of 1-O-Allyloxycarbonyl-2,3,5-tri-O-benzyl-4-O-<2,4-di-O-acetyl-3-O-<2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranosyl>-D-ribitol

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Technology Process of 1-O-Allyloxycarbonyl-2,3,5-tri-O-benzyl-4-O-<2,4-di-O-acetyl-3-O-<2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranosyl>-D-ribitol

There total 1 articles about 1-O-Allyloxycarbonyl-2,3,5-tri-O-benzyl-4-O-<2,4-di-O-acetyl-3-O-<2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranosyl>-D-ribitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: Carbonic acid allyl ester (2S,3S,4R)-2,3,4-tris-benzyloxy-4-hydroxy-butyl ester

: 131328-65-9
2,4-Di-O-acetyl-3-O-<2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranosyl trichloroacetimidate

: 131328-68-2
1-O-Allyloxycarbonyl-2,3,5-tri-O-benzyl-4-O-<2,4-di-O-acetyl-3-O-<2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranosyl>-D-ribitol

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at -30 ℃; for 0.0833333h;
DOI:10.1016/0008-6215(90)84051-U

Reference yield: 82.0%

: 131328-68-2
1-O-Allyloxycarbonyl-2,3,5-tri-O-benzyl-4-O-<2,4-di-O-acetyl-3-O-<2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranosyl>-D-ribitol

: 131328-69-3
2,3,5-Tri-O-benzyl-4-O-<2,4-di-O-acetyl-3-O-<2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranosyl>-D-ribitol

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; for 2.5h; Heating;
DOI:10.1016/0008-6215(90)84051-U

Reference yield:

: 131328-68-2
1-O-Allyloxycarbonyl-2,3,5-tri-O-benzyl-4-O-<2,4-di-O-acetyl-3-O-<2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranosyl>-D-ribitol

: C₄₄H₆₀O₁₉

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / Pd(Ph₃P)4 / tetrahydrofuran / 2.5 h / Heating

2: 100 percent / NaOMe / methanol / Ambient temperature

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium methylate; In tetrahydrofuran; methanol;
DOI:10.1016/0008-6215(90)84051-U