C₁₆H₁₈N₂O*ClH

Base Information

Chemical Name:C₁₆H₁₈N₂O*ClH
CAS No.:1333114-75-2
Molecular Formula:C₁₆H₁₈N₂O*ClH
Molecular Weight:290.793
Hs Code.:

C<sub>16</sub>H<sub>18</sub>N<sub>2</sub>O*ClH

Synonyms:C₁₆H₁₈N₂O*ClH

Suppliers and Price of C₁₆H₁₈N₂O*ClH

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₆H₁₈N₂O*ClH

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₆H₁₈N₂O*ClH

There total 7 articles about C₁₆H₁₈N₂O*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1333114-74-1
C₂₁H₂₆N₂O₃

: 1333114-75-2
C₁₆H₁₈N₂O*ClH

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 20 ℃; for 1h;

Reference yield:

: 38749-79-0
3-bromo-2-picoline

: 1333114-75-2
C₁₆H₁₈N₂O*ClH

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-Bromosuccinimide / dibenzoyl peroxide / tetrachloromethane / 4 h / Reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 - 20 °C

2.2: 16 h / 20 °C

3.1: triethylamine / 1,3-bis-(diphenylphosphino)propane; palladium diacetate / 30 h / 120 °C / 7500.75 Torr

4.1: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 - 20 °C

5.1: N-Bromosuccinimide; triphenylphosphine / tetrahydrofuran / 2 h / 0 - 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 24 h / 0 - 20 °C

7.1: hydrogenchloride / ethyl acetate / 1 h / 20 °C

With hydrogenchloride; N-Bromosuccinimide; lithium aluminium tetrahydride; sodium hydride; triethylamine; triphenylphosphine; 1,3-bis-(diphenylphosphino)propane; palladium diacetate; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; diethyl ether; ethyl acetate; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 754131-60-7
3-bromo-2-(bromomethyl)pyridine

: 1333114-75-2
C₁₆H₁₈N₂O*ClH

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 - 20 °C

1.2: 16 h / 20 °C

2.1: triethylamine / 1,3-bis-(diphenylphosphino)propane; palladium diacetate / 30 h / 120 °C / 7500.75 Torr

3.1: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 - 20 °C

4.1: N-Bromosuccinimide; triphenylphosphine / tetrahydrofuran / 2 h / 0 - 20 °C

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 24 h / 0 - 20 °C

6.1: hydrogenchloride / ethyl acetate / 1 h / 20 °C

With hydrogenchloride; N-Bromosuccinimide; lithium aluminium tetrahydride; sodium hydride; triethylamine; triphenylphosphine; 1,3-bis-(diphenylphosphino)propane; palladium diacetate; In tetrahydrofuran; diethyl ether; ethyl acetate; N,N-dimethyl-formamide; mineral oil;