N₁-n-butyl-N₂-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)oxalamide

Base Information

Chemical Name:N₁-n-butyl-N₂-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)oxalamide
CAS No.:1402547-93-6
Molecular Formula:C₃₄H₅₂N₂O₃Si
Molecular Weight:564.884
Hs Code.:

N<sub>1</sub>-n-butyl-N<sub>2</sub>-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)oxalamide

Synonyms:N₁-n-butyl-N₂-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)oxalamide

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Chemical Property of N₁-n-butyl-N₂-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)oxalamide

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Technology Process of N₁-n-butyl-N₂-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)oxalamide

There total 7 articles about N₁-n-butyl-N₂-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)oxalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 29262-59-7
2-(n-butylamino)-2-oxoacetic acid

: 1402547-85-6
1-tert-butyldiphenylsilyloxy-12-aminododec-7(Z)-ene

: 1402547-93-6
N₁-n-butyl-N₂-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)oxalamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 1402547-82-3
12-(tert-butyldiphenylsilyloxy)dodec-5-yn-1-ol

: 1402547-93-6
N₁-n-butyl-N₂-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)oxalamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen; sodium tetrahydroborate / ethylenediamine; nickel(II) acetate tetrahydrate / ethanol / 1 h

2.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.67 h / -20 °C / Inert atmosphere

2.2: 4 h / 0 - 20 °C

3.1: triphenylphosphine; water / tetrahydrofuran / 12 h

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

With sodium tetrahydroborate; di-isopropyl azodicarboxylate; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; nickel(II) acetate tetrahydrate; ethylenediamine; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 622842-63-1
tert-butyldiphenyl-[(12-(tetrahydro-2H-pyran-2-yloxy)dodec-7-ynyloxy)]silane

: 1402547-93-6
N₁-n-butyl-N₂-(12-(tert-butyldiphenylsilyloxy)dodec-5(Z)-enyl)oxalamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanol / toluene-4-sulfonic acid / 10 h / 20 °C

2.1: hydrogen; sodium tetrahydroborate / ethylenediamine; nickel(II) acetate tetrahydrate / ethanol / 1 h

3.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.67 h / -20 °C / Inert atmosphere

3.2: 4 h / 0 - 20 °C

4.1: triphenylphosphine; water / tetrahydrofuran / 12 h

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

With methanol; sodium tetrahydroborate; di-isopropyl azodicarboxylate; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; nickel(II) acetate tetrahydrate; toluene-4-sulfonic acid; ethylenediamine; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;