(E)-N'-(1-(2-chlorophenyl)-3-(p-tolyl)but-3-en-1-ylidene)-4-nitrobenzenesulfonohydrazide

Base Information

Chemical Name:(E)-N'-(1-(2-chlorophenyl)-3-(p-tolyl)but-3-en-1-ylidene)-4-nitrobenzenesulfonohydrazide
CAS No.:1613246-95-9
Molecular Formula:C₂₃H₂₀ClN₃O₄S
Molecular Weight:469.948
Hs Code.:

Synonyms:(E)-N'-(1-(2-chlorophenyl)-3-(p-tolyl)but-3-en-1-ylidene)-4-nitrobenzenesulfonohydrazide

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Chemical Property of (E)-N'-(1-(2-chlorophenyl)-3-(p-tolyl)but-3-en-1-ylidene)-4-nitrobenzenesulfonohydrazide

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Technology Process of (E)-N'-(1-(2-chlorophenyl)-3-(p-tolyl)but-3-en-1-ylidene)-4-nitrobenzenesulfonohydrazide

There total 5 articles about (E)-N'-(1-(2-chlorophenyl)-3-(p-tolyl)but-3-en-1-ylidene)-4-nitrobenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 2937-05-5
4-nitrobenzenesulfonohydrazide

: 1613247-54-3
1-(2-chlorophenyl)-3-(p-tolyl)but-3-en-1-one

: 1613246-95-9
(E)-N'-(1-(2-chlorophenyl)-3-(p-tolyl)but-3-en-1-ylidene)-4-nitrobenzenesulfonohydrazide

Guidance literature:: With ethanol; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ol5013982

Reference yield:

: 65374-22-3
1-(3-bromoprop-1-en-2-yl)-4-methylbenzene

: 1613246-95-9
(E)-N'-(1-(2-chlorophenyl)-3-(p-tolyl)but-3-en-1-ylidene)-4-nitrobenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran; water / 48 h / 50 °C / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 3 h / 0 °C / Inert atmosphere

3: ethanol / 48 h / 20 °C / Inert atmosphere

With ethanol; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ol5013982

Reference yield:

: 1613247-39-4
1-(2-chlorophenyl)-3-(p-tolyl)but-3-en-1-ol

: 1613246-95-9
(E)-N'-(1-(2-chlorophenyl)-3-(p-tolyl)but-3-en-1-ylidene)-4-nitrobenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: Dess-Martin periodane / dichloromethane / 3 h / 0 °C / Inert atmosphere

2: ethanol / 48 h / 20 °C / Inert atmosphere

With ethanol; Dess-Martin periodane; In dichloromethane;
DOI:10.1021/ol5013982