allyl (5R,6S)-3-[4-({[(methylamino)-carbonyl]-amino}-methyl)-phenyl]-7-oxo-6-{(1R)-1-[(trimethylsilyl)-oxy]-ethyl}-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

Base Information

• Chemical Name: allyl (5R,6S)-3-[4-({[(methylamino)-carbonyl]-amino}-methyl)-phenyl]-7-oxo-6-{(1R)-1-[(trimethylsilyl)-oxy]-ethyl}-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate
• CAS No.: 524072-33-1
• Molecular Formula: C₂₄H₃₃N₃O₅Si
• Molecular Weight: 471.629

Synonyms:allyl (5R,6S)-3-[4-({[(methylamino)-carbonyl]-amino}-methyl)-phenyl]-7-oxo-6-{(1R)-1-[(trimethylsilyl)-oxy]-ethyl}-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

Chemical Property of allyl (5R,6S)-3-[4-({[(methylamino)-carbonyl]-amino}-methyl)-phenyl]-7-oxo-6-{(1R)-1-[(trimethylsilyl)-oxy]-ethyl}-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

Chemical Property:

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Technology Process of allyl (5R,6S)-3-[4-({[(methylamino)-carbonyl]-amino}-methyl)-phenyl]-7-oxo-6-{(1R)-1-[(trimethylsilyl)-oxy]-ethyl}-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

There total 1 articles about allyl (5R,6S)-3-[4-({[(methylamino)-carbonyl]-amino}-methyl)-phenyl]-7-oxo-6-{(1R)-1-[(trimethylsilyl)-oxy]-ethyl}-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

allyl ((2R,3S)-2-{2-[4-({[(methylamino)-carbonyl]-amino}-methyl)-phenyl]-2-oxoethyl}-4-oxo-3-{(1R)-1-[(trimethylsilyl)-oxy]-ethyl}-azetidin-1-yl) (triphenylphosphoranilidene) acetate (524071-54-3) → allyl (5R,6S)-3-[4-({[(methylamino)-carbonyl]-amino}-methyl)-phenyl]-7-oxo-6-{(1R)-1-[(trimethylsilyl)-oxy]-ethyl}-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate (524072-33-1)

Guidance literature:

With bistrimethylsilylamide; In 1,4-dioxane; toluene; for 6h; Heating / reflux;

Reference yield:

allyl (5R,6S)-3-[4-({[(methylamino)-carbonyl]-amino}-methyl)-phenyl]-7-oxo-6-{(1R)-1-[(trimethylsilyl)-oxy]-ethyl}-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate (524072-33-1) → C21H25N3O5

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; at 0 ℃; for 1h; pH=2.5;

upstream raw materials:

allyl ((2R,3S)-2-{2-[4-({[(methylamino)-carbonyl]-amino}-methyl)-phenyl]-2-oxoethyl}-4-oxo-3-{(1R)-1-[(trimethylsilyl)-oxy]-ethyl}-azetidin-1-yl) (triphenylphosphoranilidene) acetate

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