1-Dimethylamino-2-nitro-3-phenyl-4-(α-hydroxy-4-nitro-benzyl)-cyclobuten

Base Information

Chemical Name:1-Dimethylamino-2-nitro-3-phenyl-4-(α-hydroxy-4-nitro-benzyl)-cyclobuten
CAS No.:5530-06-3
Molecular Formula:C₁₉H₁₉N₃O₅
Molecular Weight:369.377
Hs Code.:

Synonyms:1-Dimethylamino-2-nitro-3-phenyl-4-(α-hydroxy-4-nitro-benzyl)-cyclobuten

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Chemical Property of 1-Dimethylamino-2-nitro-3-phenyl-4-(α-hydroxy-4-nitro-benzyl)-cyclobuten

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Technology Process of 1-Dimethylamino-2-nitro-3-phenyl-4-(α-hydroxy-4-nitro-benzyl)-cyclobuten

There total 4 articles about 1-Dimethylamino-2-nitro-3-phenyl-4-(α-hydroxy-4-nitro-benzyl)-cyclobuten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 340-01-2
4,4-dichloro-3,3-difluoro-1-phenyl-cyclobutene

: 5530-06-3
1-Dimethylamino-2-nitro-3-phenyl-4-(α-hydroxy-4-nitro-benzyl)-cyclobuten

Guidance literature:: Multi-step reaction with 4 steps

1: NaNO₂, urea, benzene-1,2-diol / dimethylformamide

2: H₂, CaCO₃ / Pd-C / methanol

3: CHCl₃

4: KOtBu / dimethylsulfoxide

With potassium tert-butylate; hydrogen; benzene-1,2-diol; urea; calcium carbonate; sodium nitrite; palladium on activated charcoal; In methanol; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja00950a027

Reference yield:

: 5530-00-7
1-Phenyl-2-chlor-3,3-difluor-4-nitro-cyclobuten

: 5530-06-3
1-Dimethylamino-2-nitro-3-phenyl-4-(α-hydroxy-4-nitro-benzyl)-cyclobuten

Guidance literature:: Multi-step reaction with 3 steps

1: H₂, CaCO₃ / Pd-C / methanol

2: CHCl₃

3: KOtBu / dimethylsulfoxide

With potassium tert-butylate; hydrogen; calcium carbonate; palladium on activated charcoal; In methanol; chloroform; dimethyl sulfoxide;
DOI:10.1021/ja00950a027

Reference yield:

: 4919-60-2
1,1-Difluor-2-nitro-3-phenyl-cyclobutan

: 5530-06-3
1-Dimethylamino-2-nitro-3-phenyl-4-(α-hydroxy-4-nitro-benzyl)-cyclobuten

Guidance literature:: Multi-step reaction with 2 steps

1: CHCl₃

2: KOtBu / dimethylsulfoxide

With potassium tert-butylate; In chloroform; dimethyl sulfoxide;
DOI:10.1021/ja00950a027