N-(7-(5,5-dimethylcyclohex-2-enyloxy)-8-methyl-2-oxo-2H-chromen-3-yl)-3',6-dimethoxybiphenyl-3-carboxamide

Base Information

Chemical Name:N-(7-(5,5-dimethylcyclohex-2-enyloxy)-8-methyl-2-oxo-2H-chromen-3-yl)-3',6-dimethoxybiphenyl-3-carboxamide
CAS No.:1160950-88-8
Molecular Formula:C₃₃H₃₃NO₆
Molecular Weight:539.628
Hs Code.:

Synonyms:N-(7-(5,5-dimethylcyclohex-2-enyloxy)-8-methyl-2-oxo-2H-chromen-3-yl)-3',6-dimethoxybiphenyl-3-carboxamide

Suppliers and Price of N-(7-(5,5-dimethylcyclohex-2-enyloxy)-8-methyl-2-oxo-2H-chromen-3-yl)-3',6-dimethoxybiphenyl-3-carboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(7-(5,5-dimethylcyclohex-2-enyloxy)-8-methyl-2-oxo-2H-chromen-3-yl)-3',6-dimethoxybiphenyl-3-carboxamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of N-(7-(5,5-dimethylcyclohex-2-enyloxy)-8-methyl-2-oxo-2H-chromen-3-yl)-3',6-dimethoxybiphenyl-3-carboxamide

There total 8 articles about N-(7-(5,5-dimethylcyclohex-2-enyloxy)-8-methyl-2-oxo-2H-chromen-3-yl)-3',6-dimethoxybiphenyl-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 25866-56-2
(+/-)-5,5-dimethylcyclohex-2-en-1-ol

: 1160950-71-9
C₂₅H₂₁NO₆

: 1160950-88-8
N-(7-(5,5-dimethylcyclohex-2-enyloxy)-8-methyl-2-oxo-2H-chromen-3-yl)-3',6-dimethoxybiphenyl-3-carboxamide

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 ℃; for 2h;
DOI:10.1021/jm200148p

Reference yield:

: 1083313-05-6
3′,6-dimethoxy-[1,1′-biphenyl]-3-carboxylic acid

: 1160950-88-8
N-(7-(5,5-dimethylcyclohex-2-enyloxy)-8-methyl-2-oxo-2H-chromen-3-yl)-3',6-dimethoxybiphenyl-3-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / tetrahydrofuran

2: triethylamine / tetrahydrofuran

3: triethylamine / methanol

4: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 0 °C

With thionyl chloride; di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; 4: Mitsunobu reaction;
DOI:10.1021/jm200148p

Reference yield:

: 1083313-80-7
3',6-dimethoxy-[1,1'-biphenyl]-3-carbonyl chloride

: 1160950-88-8
N-(7-(5,5-dimethylcyclohex-2-enyloxy)-8-methyl-2-oxo-2H-chromen-3-yl)-3',6-dimethoxybiphenyl-3-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran

2: triethylamine / methanol

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 0 °C

With di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; 3: Mitsunobu reaction;
DOI:10.1021/jm200148p