3-Benzo[1,3]dioxol-5-yl-N-{3-[{4-[[3-(3-benzo[1,3]dioxol-5-yl-propionylamino)-propyl]-(toluene-4-sulfonyl)-amino]-butyl}-(toluene-4-sulfonyl)-amino]-propyl}-propionamide

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Chemical Name:3-Benzo[1,3]dioxol-5-yl-N-{3-[{4-[[3-(3-benzo[1,3]dioxol-5-yl-propionylamino)-propyl]-(toluene-4-sulfonyl)-amino]-butyl}-(toluene-4-sulfonyl)-amino]-propyl}-propionamide
CAS No.:96917-51-0
Molecular Formula:C₄₄H₅₄N₄O₁₀S₂
Molecular Weight:863.066
Hs Code.:

3-Benzo[1,3]dioxol-5-yl-N-{3-[{4-[[3-(3-benzo[1,3]dioxol-5-yl-propionylamino)-propyl]-(toluene-4-sulfonyl)-amino]-butyl}-(toluene-4-sulfonyl)-amino]-propyl}-propionamide

Synonyms:3-Benzo[1,3]dioxol-5-yl-N-{3-[{4-[[3-(3-benzo[1,3]dioxol-5-yl-propionylamino)-propyl]-(toluene-4-sulfonyl)-amino]-butyl}-(toluene-4-sulfonyl)-amino]-propyl}-propionamide

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Chemical Property of 3-Benzo[1,3]dioxol-5-yl-N-{3-[{4-[[3-(3-benzo[1,3]dioxol-5-yl-propionylamino)-propyl]-(toluene-4-sulfonyl)-amino]-butyl}-(toluene-4-sulfonyl)-amino]-propyl}-propionamide

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Technology Process of 3-Benzo[1,3]dioxol-5-yl-N-{3-[{4-[[3-(3-benzo[1,3]dioxol-5-yl-propionylamino)-propyl]-(toluene-4-sulfonyl)-amino]-butyl}-(toluene-4-sulfonyl)-amino]-propyl}-propionamide

There total 6 articles about 3-Benzo[1,3]dioxol-5-yl-N-{3-[{4-[[3-(3-benzo[1,3]dioxol-5-yl-propionylamino)-propyl]-(toluene-4-sulfonyl)-amino]-butyl}-(toluene-4-sulfonyl)-amino]-propyl}-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 110-52-1
1,4-dibromo-butane

: 96917-50-9
3-Benzo[1,3]dioxol-5-yl-N-[3-(toluene-4-sulfonylamino)-propyl]-propionamide

: 96917-51-0
3-Benzo[1,3]dioxol-5-yl-N-{3-[{4-[[3-(3-benzo[1,3]dioxol-5-yl-propionylamino)-propyl]-(toluene-4-sulfonyl)-amino]-butyl}-(toluene-4-sulfonyl)-amino]-propyl}-propionamide

Guidance literature:: With potassium carbonate; In chloroform; for 24h; Heating;

Reference yield:

: 10431-93-3
2-methyl-(4H)-5,6-dihydro-1,3-oxazine

: 96917-51-0
3-Benzo[1,3]dioxol-5-yl-N-{3-[{4-[[3-(3-benzo[1,3]dioxol-5-yl-propionylamino)-propyl]-(toluene-4-sulfonyl)-amino]-butyl}-(toluene-4-sulfonyl)-amino]-propyl}-propionamide

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) LDA / 1.) THF, -78 deg C, 1 h, 2.) THF, from -78 deg C to RT, 0.5 h

2: Me₃SiN₃, methanol / dimethylformamide / 4 h / 60 °C

3: 97 percent / H₂ / Lindlar catalyst / ethanol / 0.5 h / Ambient temperature

4: 82 percent / Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

5: 97 percent / K₂CO₃ / CHCl₃ / 24 h / Heating

With methanol; trimethylsilylazide; hydrogen; potassium carbonate; triethylamine; lithium diisopropyl amide; Lindlar's catalyst; In ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide;

Reference yield:

: 25054-53-9
3,4-(methylenedioxy)benzoyl chloride

: 96917-51-0
3-Benzo[1,3]dioxol-5-yl-N-{3-[{4-[[3-(3-benzo[1,3]dioxol-5-yl-propionylamino)-propyl]-(toluene-4-sulfonyl)-amino]-butyl}-(toluene-4-sulfonyl)-amino]-propyl}-propionamide

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) LDA / 1.) THF, -78 deg C, 1 h, 2.) THF, from -78 deg C to RT, 0.5 h

2: Me₃SiN₃, methanol / dimethylformamide / 4 h / 60 °C

3: 97 percent / H₂ / Lindlar catalyst / ethanol / 0.5 h / Ambient temperature

4: 82 percent / Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

5: 97 percent / K₂CO₃ / CHCl₃ / 24 h / Heating

With methanol; trimethylsilylazide; hydrogen; potassium carbonate; triethylamine; lithium diisopropyl amide; Lindlar's catalyst; In ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide;